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Pd- : / PROCESS FOR Pd-CATALYZED HYDROXYCARBONYLATION OF DIISOBUTENE: ACETIC ACID/DIISOBUTENE RATIO
Pd- : / PROCESS FOR Pd-CATALYZED HYDROXYCARBONYLATION OF DIISOBUTENE: ACETIC ACID/DIISOBUTENE RATIO
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机译:Pd-:/ Pd催化双异丁烯羟基羰基化的方法:乙酸/二异丁烯比例
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摘要
The present invention relates to a method for Pd-catalyzed hydroxycarbonylation of diisobutene (DIBN): acetic acid/DIBN ratio. The present invention is to provide an excellent conversion ratio in Pd-catalyzed hydroxycarbonylation of DIBN. The method comprises the following steps of: a) adding DIBN; b) adding a compound including Pd which can form a complex; c) adding a ligand L1; d) adding 5 to 8 mol of acetic acid per mol of DIBN; e) supplying CO; and f) heating the reactive mixture and converting DIBN into a compound P1.
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