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Process for the preparation of high purity iridium (III) chloride hydrate
Process for the preparation of high purity iridium (III) chloride hydrate
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机译:制备高纯度氯化铱(III)水合物的方法
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摘要
As a process for producing high purity iridium (III) chloride hydrate, (1) solid H 2 comprising the steps of: providing at least one material selected from the [IrCl 6] hydrate, 1 wt% or more H 2 [IrCl 6] aqueous solution, and solid tetrahydrate IrCl group consisting of; (2) The molar ratio of monohydroxy compound miscible with water in any ratio, primary monoalcohol containing 4 to 6 carbon atoms, and Ir (IV): monohydroxy compound is 1: 0.6 to 1000 One or more monohydroxy compounds selected from the group consisting of secondary monoalcohols containing from 4 to 6 carbon atoms are added to the one or more materials provided in step (1) and are 0.2 to 48 in a temperature range of 20 to 120 ° C. Allowing to react for a time and then removing the volatile components from the reaction mixture formed therefrom.
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