首页> 外国专利> SIMULATOR OF THE SIGNALS OF FREE PRECESSION OF NUCLEAR MAGNETIC RESONANCE AND SPIN ECHO OF OIL PROTONS WITH VARIOUS MASS FRACTIONS OF LINOLENIC ACID IN LINSEEDS

SIMULATOR OF THE SIGNALS OF FREE PRECESSION OF NUCLEAR MAGNETIC RESONANCE AND SPIN ECHO OF OIL PROTONS WITH VARIOUS MASS FRACTIONS OF LINOLENIC ACID IN LINSEEDS

机译:亚麻仁中不同质量分数的油质子核磁共振自由前趋和油质子自旋回旋信号的模拟

摘要

FIELD: measurement.;SUBSTANCE: invention relates to the field of measurement equipment, namely to means of calibrating pulse NMR-spectrometers, and can be used to determine content of linolenic acid in linseed oil. Invention is a simulator of free precession signals of nuclear magnetic resonance and spin echo of oil protons with different mass fraction of linolenic acid in flax seeds, which is a first organosilicon liquid or a mixture of organosilicon liquids having spin-spin relaxation time of protons in different ranges, characterized in that the first liquid has a spin-spin relaxation time of protons in range of 240±10 ms, and second is in range of 200±10 ms at their following ratio, wt. %: first organosilicon liquid 14.3–100.0; second organosilicon liquid is 0–85.7. Claimed ratios of said organosilicon fluids enable to simulate spin envelope signals of protons of linseed oil with weight ratio of linolenic acid in range from 4 to 72 %.;EFFECT: flax seed oil simulators can be used in making reference measures for calibrating and calibrating NMR analyzers of oil content and moisture of seeds.;1 cl, 1 tbl, 1 ex
机译:脉冲核磁共振波谱仪的校准装置技术领域本发明涉及测量设备领域,即涉及一种脉冲核磁共振波谱仪的校准方法,可用于测定亚麻子油中亚麻酸的含量。本发明是一种具有核磁共振自由进动信号和亚麻籽中具有不同质量分数的亚麻酸的油质子自旋回波的模拟器,其是质子自旋自旋弛豫时间为1的第一有机硅液体或有机硅液体的混合物。在不同的范围内,其特征在于,第一液体的质子自旋自旋弛豫时间在240±10 ms的范围内,第二液体在其随后的重量比wt。下在200±10 ms的范围内。 %:第一有机硅液体14.3–100.0;第二种有机硅液体为0-85.7。声称的所述有机硅流体的比例能够模拟亚麻籽油质子的自旋包络信号,亚麻酸的重量比范围为4至72%.;效果:亚麻籽油模拟器可用于校准和校准NMR的参考措施种子含油量和水分的分析仪。; 1 cl,1 tbl,1 ex

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