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Method for preparing flame-retardant and melt droplet-resistant polyester

机译:阻燃耐熔滴聚酯的制备方法

摘要

A method for preparing flame-retardant melt droplet-resistant polyester, consisting of the following steps: A) uniformly mixing four materials consisting of flame-retardant melt droplet-resistant basic magnesium sulfate whiskers, beta-type silicon nitride whiskers, tetra-needle like zinc oxide whiskers and magnesium salt whiskers; roasting in a vacuum furnace; stirring and dispersing in a sodium hexametaphosphate solution, treating by atmospheric-pressure plasma; filtering through a 200 mesh filter and drying; B) mixing the whiskers obtained from the step A) with flame retardant agents and a silane coupling agent at 75°C, where the flame retardant agents are melamine cyanurate (MCA) and microencapsulated red phosphorus; C) preparing a flame-retardant melt droplet-resistant whiskers ethylene glycol solution using the flame-retardant melt droplet-resistant whiskers obtained in the step B); D) preparing a flame-retardant melt droplet-resistant polyester from the flame-retardant melt droplet-resistant whiskers in a blending or copolyester manner, and preparing a sheath-core flame-retardant melt droplet-resistant polyester thread by means of compound spinning technology, where the surface layer of the thread is the flame-retardant melt droplet-resistant polyester.
机译:一种阻燃耐熔滴聚酯的制备方法,其包括以下步骤:a)将阻燃耐熔滴碱性硫酸镁晶须,β型氮化硅晶须,四针状四针组成的四种材料均匀混合。氧化锌晶须和镁盐晶须;在真空炉中烘烤;搅拌分散于六偏磷酸钠溶液中,用大气压等离子体处理。通过200目过滤器过滤并干燥; B)将步骤A)中获得的晶须与阻燃剂和硅烷偶联剂在75°C下混合,其中阻燃剂为三聚氰胺三聚氰胺(MCA)和微囊化的红磷; C)使用步骤B)中获得的阻燃性耐熔滴晶须制备乙二醇溶液。 D)由阻燃性抗熔滴晶须以共混或共聚酯的方式制备阻燃性抗熔滴聚脂,并通过复合纺丝技术制备皮芯阻燃性抗熔滴性涤纶线,其中线的表面层是阻燃的抗熔滴聚酯。

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