Station for electrochemical measurements in the environment of melted salts in high-temperature conditions

摘要

the electrochemical measurements in the environment of molten salts in high-temperature conditions, especially in the working conditions of molten carbonate fuel cells.contains electric furnace (1) equipped with the steel kwasoodpornej, with elements in the form of spiral grzejnymi placed in shielding materials porcelain and sheathed in additionfrom the housing, a thermal insulation.inside a furnace (1) is placed the crucible or the reactor (18) with alumina, which, in turn, are placed inside the electrodes (17) of a material resistant to high temperatures.combined with the electric conductors (14) to elektroanalitycznych measurements and is placed termopara (15) for measuring the temperature inside the crucible or reactor (18).an electric furnace (1) has a cylindrical shape, and the heating elements are placed on the circumference around the crucible or reactor (18).the furnace (1) is closed from the top lid (9), in which openings located over the crucible or reactor (18) are mounted vertically sections of pipe fittings of aluminium oxide.in which are placed parts electrical wiring electrodes (17) connecting the electrodes of the measurement elektroanalitycznych (14), and is placed termopara (15).the side wall (1) is mounted a furnace tubing with alumina, which is placed termopara (16) for measuring the temperature inside the furnace (1).the furnace (1) is connected with the power source via the circuits (2) connected to a current intensity (3) equipped with a tension gauge.cabinet (2) is equipped with a thermal regulator (12), the temperature inside the furnace (1),combined with termoparą (16) for measuring the temperature inside the furnace (1) and a thermoregulator (13) temperature inside the crucible or reactor (18),combined with termoparą (15) for measuring the temperature inside the crucible or reactor (18).