首页> 外国专利> New ionic liquids with L-lactate anion and N-alkyltebuconazole cation, method of their production and use as compounds inhibiting the development of mycelium

New ionic liquids with L-lactate anion and N-alkyltebuconazole cation, method of their production and use as compounds inhibiting the development of mycelium

机译:具有L-乳酸阴离子和N-烷基戊唑醇阳离子的新型离子液体,其制备方法和用作抑制菌丝体发育的化合物的方法

摘要

New ion fluids with an L-lactate anion and an N-alkyltebuconazole cation, of a general formula 1, in which R stands for an alkyl base containing from 1 to 10 carbon atoms or a benzyl base, are reported. The notification shall also include the way in which they are obtained, which consists in surrendering a fourth-grade N-alkyltebuconazole halogen of a general formula 2 in which R stands for an alkyl base containing from 1 to 10 carbon atoms or a benzyl base,in the case of continuous mixing, the reaction of anion exchange to ion resin or potassium hydroxide, or sodium hydroxide in relation to molar quartz salt to the hydroxyl ion donor 1:1, in a solvent of the alcohol group: methanol or ethanol, at a temperature of 25 to 30,C, preferably 20,C, After the solvent has been removed from the solvent, the ion resin with adsorbed halogen ions or an inorganic by-product is removed, the transfer is subjected to an anaesthetic reaction with L-lactic acid, at a temperature from 20 to 30, then evaporate the solvent,and the resulting product is drying under a reduced temperature pressure from 30-to 60-degrees, preferably 40-degrees. The purpose of the notification is also to use L-lactates of N-alkylotebuconazole with a general formula 1, in which R stands for an alkyl base containing from 1 to 10 carbon atoms or benzyl as a fungal inhibitory agent.
机译:据报道,具有L-乳酸阴离子和N-烷基戊康唑阳离子的新型离子流体,其中R代表含有1至10个碳原子的烷基或苄基。通知还应包括获得它们的方式,该方式包括交出通式2的四级N-烷基tebuconazole卤素,其中R代表含1至10个碳原子的烷基或苄基,在连续混合的情况下,在醇基的溶剂:甲醇或乙醇中,阴离子交换剂与离子树脂或氢氧化钾或氢氧化钠(相对于摩尔石英盐)与羟基离子供体的比例为1:1:温度为25至30°C,最好为20°C。从溶剂中除去溶剂后,除去吸附有卤素离子或无机副产物的离子树脂,然后将转移液与L进行麻醉反应。 -乳酸在20至30的温度下,然后蒸发溶剂,并且所得产物在30至60度,优选40度的减压下干燥。该通报的目的还在于使用具有通式1的N-烷基奥特康唑的L-乳酸酯,其中R代表含有1至10个碳原子的烷基碱或苄基作为真菌抑制剂。

著录项

  • 公开/公告号PL426060A1

    专利类型

  • 公开/公告日2020-01-02

    原文格式PDF

  • 申请/专利权人 POLITECHNIKA POZNAŃSKA;

    申请/专利号PL20180426060

  • 发明设计人 JULIUSZ PERNAK;DARIA CZURYSZKIEWICZ;

    申请日2018-06-25

  • 分类号C07D249/08;A01N43/653;A01P3;

  • 国家 PL

  • 入库时间 2022-08-21 11:16:27

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