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METHOD FOR SYNTHESIZING AN AFX-STRUCTURE ZEOLITE FROM A MIXTURE OF FAU ZEOLITES IN THE PRESENCE OF AN ORGANIC NITROGEN-CONTAINING STRUCTURING AGENT
METHOD FOR SYNTHESIZING AN AFX-STRUCTURE ZEOLITE FROM A MIXTURE OF FAU ZEOLITES IN THE PRESENCE OF AN ORGANIC NITROGEN-CONTAINING STRUCTURING AGENT
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机译:存在有机氮结构剂的情况下,由多种沸石合成AFX结构沸石的方法
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摘要
The invention relates to a method for preparing an AFX-structure zeolite, said method comprising at least the following steps: i) in an aqueous medium, mixing at least two FAU-structure zeolites, each of said FAU-structure zeolites having a molar ratio SiO2/Al2O3 of between 2 and 200 inclusive, and a parameter Pze less than 3250, an organic nitrogen-containing compound R, at least one source of at least one alkali and/or alkaline-earth metal M, the reaction mixture having the following molar composition: (SiO2(FAU))/(Al2O3(FAU)) of between 2 and 32, H2O/(SiO2(FAU)) of between 1 and 100, R/(SiO2(FAU)) of between 0.01 and 0.6, M2/nO/(SiO2(FAU)) of between 0.005 and 0.45, limits included, in order to obtain a homogeneous precursor gel; and ii) subjecting the precursor gel resulting from step (i) to hydrothermal treatment.
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机译:本发明涉及一种制备AFX结构沸石的方法,所述方法至少包括以下步骤:i)在水性介质中,混合至少两种FAU结构沸石,每种所述FAU结构沸石具有摩尔比。 SiO 2 Sub> / Al 2 Sub> O 3 Sub>在2到200之间,且参数P ze Sub>小于3250 ,有机含氮化合物R,至少一种碱金属和/或碱土金属M的至少一种来源,反应混合物具有以下摩尔组成:(SiO 2 Sub> ( FAU) Sub>)/(Al 2 Sub> O 3 Sub> (FAU) Sub>)介于2和32之间,H 2 < / Sub> O /(SiO 2 Sub> (FAU) Sub>)介于1和100之间,R /(SiO 2 Sub> (FAU) Sub>)在0.01和0.6之间,M 2 / n Sub> O /(SiO 2 Sub> (FAU) Sub>)在0.005和0.45之间为了获得均质的前体凝胶,包括了限值; ii)对步骤(i)所得的前体凝胶进行水热处理。
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