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METHOD FOR PREPARING REDUCED GRAPHENE OXIDE-BASED COMPOSITE FILM

机译:还原的氧化石墨烯基复合膜的制备方法

摘要

Disclosed in the present invention is a method for preparing a reduced graphene oxide-based composite film. The method uses graphene oxide as a raw material, which is mixed with other substances in water or another solvent, then a reduced graphene oxide-based composite film or a reduced graphene oxide-based composite gel film is prepared by means of a hydrothermal reaction or a solvothermal reaction in a closed reaction vessel, and the reduced graphene oxide-based composite gel is converted into a composite film by means of freeze drying or supercritical drying. A thinner composite film may be obtained from a synthesized composite film by means of dipping and drying in a solvent. Alternatively, a reduced graphene oxide-based composite film having a higher graphene reduction degree and a more complete crystal structure may be obtained by performing high temperature reduction on a reduced graphene oxide-based composite film.
机译:本发明公开了一种还原性氧化石墨烯系复合膜的制备方法。该方法使用氧化石墨烯作为原料,将其与其他物质在水或另一种溶剂中混合,然后通过水热反应或还原反应制备还原的氧化石墨烯基复合膜或还原的氧化石墨烯基复合凝胶膜。在密闭的反应容器中进行溶剂热反应,然后通过冷冻干燥或超临界干燥将还原的基于氧化石墨烯的复合凝胶转化为复合膜。可以通过浸渍并在溶剂中干燥而从合成的复合膜获得更薄的复合膜。或者,通过对还原性氧化石墨烯类复合膜进行高温还原,可以得到石墨烯还原度更高,晶体结构更完整的还原性氧化石墨烯类复合膜。

著录项

  • 公开/公告号WO2020146962A1

    专利类型

  • 公开/公告日2020-07-23

    原文格式PDF

  • 申请/专利权人 ZHUANG PENGYU;

    申请/专利号WO2019CN00016

  • 发明设计人 ZHUANG PENGYU;

    申请日2019-01-24

  • 分类号C01B32/184;C01B32/194;C01B33/02;B82Y30;C01B32/168;C08J5/18;C08J3/075;C08L5/08;C08K3/04;

  • 国家 WO

  • 入库时间 2022-08-21 11:10:13

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