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Process for preparing 1,4-bis (4-phenoxybenzoyl) benzene in supersaturated state
Process for preparing 1,4-bis (4-phenoxybenzoyl) benzene in supersaturated state
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机译:制备过饱和状态的1,4-双(4-苯氧基苯甲酰基)苯的方法
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摘要
The present invention is a method for producing 1,4-bis (4-phenoxybenzoyl) benzene, Providing a reaction mixture comprising terephthaloyl chloride, diphenyl ether and Lewis acid in a solvent; Reacting terephthaloyl chloride with diphenyl ether to obtain a product mixture comprising 1,4-bis (4-phenoxybenzoyl) benzene-Lewis acid complex; 1,4-bis (4-phenoxybenzoyl) benzene-Lewis acid complex during at least part of the step of reacting terephthaloyl chloride with diphenyl ether A method of dissolving in a solvent at a weight concentration of 1,4-bis (4-phenoxybenzoyl) benzene in a solvent that is higher than the saturation limit of the complex.
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