首页> 外国专利> - - Preparing method for sulfur-doped graphene using electrochemical method and bifunctional catalyst comprising sulfur-doped graphene prepared therefrom

- - Preparing method for sulfur-doped graphene using electrochemical method and bifunctional catalyst comprising sulfur-doped graphene prepared therefrom

机译:-使用电化学方法制备硫掺杂石墨烯的方法和由其制备的包含硫掺杂石墨烯的双功能催化剂

摘要

The present invention relates to a method for producing sulfur-doped graphene using electrochemical technique and a bifunctional catalyst including sulfur-doped graphene produced therefrom and, more specifically, to a sulfur-doped graphene producing method which includes: a step (1) of producing mixed solution by adding a sulfur precursor to sulfuric acid solution; a step (2) of mounting graphite foil and platinum (Pt) wire in the mixed solution produced by the step (1); a step (3) of connecting a positive (+) electrode to the graphite foil of the step (2), connecting a negative (-) electrode to the platinum wire, and separating sulfur-doped graphene by applying a voltage of 7-20 V; a step (4) of washing sulfur-doped graphene separated in the step (3); and a step (5) of performing thermal treatment after the step (4). The produced sulfur-doped graphene has a bifunctional catalytic activity in oxygen reduction reaction and oxygen generation reaction.
机译:本发明涉及一种利用电化学技术生产硫掺杂石墨烯的方法以及一种由其生产的包含硫掺杂石墨烯的双功能催化剂,更具体地,涉及一种硫掺杂石墨烯的生产方法,其包括:生产步骤(1)通过将硫前体添加到硫酸溶液中的混合溶液;步骤(2):将石墨箔和铂(Pt)线安装在步骤(1)制得的混合溶液中;步骤(3):将正(+)电极连接至步骤(2)的石墨箔,将负(-)电极连接至铂丝,并通过施加7-20的电压分离掺杂硫的石墨烯V;步骤(4)是洗涤步骤(3)中分离出的掺硫石墨烯的步骤;在步骤(4)之后进行热处理的步骤(5)。产生的硫掺杂石墨烯在氧还原反应和氧生成反应中具有双功能催化活性。

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