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METHOD FOR LOW DEFECTIVE GRAPHENE OXIDE USING ANTIOXIDANT AND GRAPHENE OXIDE THEREBY

机译:一种使用抗氧化剂和氧化石墨烯的低缺陷氧化石墨烯的方法

摘要

The present invention relates to a method for producing low defectivity graphene oxide using an oxidation stabilizer and the low defectivity graphene oxide produced by the method and, more specifically, to a graphene oxide producing method comprising: a step (a) of producing oxidation stabilizer solution by adding acid solution and an oxidation stabilizer into a reactor and stirring the same; a step (b) of adding graphite and potassium permanganate (KMnO_4) into a reactor including the oxidation stabilizer solution, and performing an oxidation reaction therein; a step (c) of obtaining a product containing graphene oxide by adding and stirring hydrogen peroxide (H_2O_2) after adding distilled water to the reactant; and a step (d) of washing and drying the product. The present invention produces low defectivity graphene oxide in which residual binding is reduced after the reduction of graphene oxide while maintaining the size of a graphene oxide sheet by suppressing the formation of a ketone group (C=O) which is a non-reducible defect formed during an oxidation process in a graphene oxide producing process.
机译:氧化石墨烯的制造方法技术领域本发明涉及一种使用氧化稳定剂的低缺陷性氧化石墨烯的制造方法以及通过该方法制造的低缺陷性氧化石墨烯的制造方法,更具体地说,涉及一种包括:氧化稳定剂溶液的制造工序(a)。在反应器中加入酸溶液和氧化稳定剂并搅拌。步骤(b):将石墨和高锰酸钾(KMnO_4)加入到包含氧化稳定剂溶液的反应器中,并在其中进行氧化反应; (c)在将蒸馏水添加至反应物中之后,通过添加并搅拌过氧化氢(H_2O_2)来获得包含氧化石墨烯的产物的步骤;洗涤和干燥产物的步骤(d)。本发明生产低缺陷度的氧化石墨烯,其中通过抑制作为不可还原缺陷形成的酮基(C = O)的形成,在保持氧化石墨烯片的尺寸的同时保持氧化石墨烯片的尺寸的同时减少了残余结合。在氧化石墨烯生产过程中的氧化过程中。

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