首页> 外国专利> YSZ MANUFACTURING METHOD OF YTTRIA STABILIZED ZIRCONIAYSZ NANO SOL HAVING EXCELLENT DISPERSIBILITY

YSZ MANUFACTURING METHOD OF YTTRIA STABILIZED ZIRCONIAYSZ NANO SOL HAVING EXCELLENT DISPERSIBILITY

机译:具有出色分散性的氧化钇稳定氧化锆纳米溶胶的YSZ制造方法

摘要

The present invention comprises the steps of: (a) mixing ZrOCl 2 ·8H 2 O sol and Y(NO 3 ) 3 ·6H 2 O sol and adjusting the pH by adding a basic substance; (B) preparing a yttria stabilized zirconia (YSZ) nanoparticles by hydrothermal reaction of the sol obtained in step (a); And (c) the step of performing a treatment for improving the dispersibility of the nano-sol dispersed in the yttria-stabilized zirconia nanoparticles; as a method for producing a yttria-stabilized zirconia nanosol having excellent dispersibility, the present invention According to the present invention, yttria stabilized zirconia (YSZ) sol having excellent dispersibility is prepared by adding various silane coupling agents, acids/bases, polymers and surfactants to nano-sized yttria stabilized zirconia (YSZ) synthesized through hydrothermal reaction. By doing so, by solving the agglomeration problem that has been pointed out as a problem in the application of nano-sized yttria-stabilized zirconia (YSZ), it is possible to exhibit more excellent physical properties when applied as a heat shield coating material.
机译:本发明包括以下步骤:(a)混合ZrOCl 2 ·8H 2 O溶胶和Y(NO 3 3 ·6H 2 O溶胶并通过添加碱性物质来调节pH值; (B)通过步骤(a)中获得的溶胶的水热反应制备氧化钇稳定的氧化锆(YSZ)纳米颗粒;并且(c)进行用于改善分散在氧化钇稳定的氧化锆纳米粒子中的纳米溶胶的分散性的处理的步骤;作为制备具有优异分散性的氧化钇稳定的氧化锆纳米溶胶的方法,本发明根据本发明,通过添加各种硅烷偶联剂,酸/碱,聚合物和表面活性剂来制备具有优异分散性的氧化钇稳定的氧化锆(YSZ)溶胶。通过水热反应合成纳米级氧化钇稳定的氧化锆(YSZ)。通过这样做,通过解决在纳米尺寸的氧化钇稳定的氧化锆(YSZ)的应用中已经指出的结块问题,当用作隔热涂层材料时,可以表现出更优异的物理性能。

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