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- - Preparation method of N-doped graphene preparation method of Sulfur-graphene composite and anode of Lithium-Sulfur battery comprising the same

机译:--硫-石墨烯复合物的n掺杂石墨烯的制备方法以及包括该方法的锂硫电池的负极

摘要

Dispersion containing graphite passes through the inlet and outlet and the microchannel of the High Pressure Homogenizer (HPH) including a microchannel having a diameter of micrometers, which connects between the inlet and the outlet and the outlet A first step of obtaining a graphene flake by peeling the graphite through a high pressure homogenizing to; Filtering and drying the obtained graphene flakes, and then putting the ammonium compound into a ball mill and performing dry ball milling under an inert atmosphere to obtain particles in which the ammonium compound is surrounded on the surface of the graphene flakes; And a third step of thermally treating the obtained particles to obtain graphene doped with nitrogen atoms; a method for preparing nitrogen-doped graphene, a method for preparing a sulfur-graphene composite using the same, comprising the sulfur-graphene composite A lithium sulfur battery positive electrode, and a lithium sulfur battery including the positive electrode are provided.
机译:包含石墨的分散液穿过高压均质器(HPH)的入口和出口以及微通道,高压均质器包括直径为微米的微通道,该微通道连接到入口和出口与出口之间。通过剥离获得石墨烯薄片的第一步石墨通过高压均质化;将得到的石墨烯薄片过滤干燥,然后将铵化合物放入球磨机中,在惰性气氛下进行干式球磨,得到在石墨烯薄片的表面包围有铵化合物的粒子。第三步,热处理所得颗粒,得到掺杂氮原子的石墨烯。本发明提供了一种制备氮掺杂石墨烯的方法,一种使用该方法制备硫石墨烯复合物的方法,该方法包括:锂硫电池正极,以及包括该正极的锂硫电池。

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