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Method for manufacturing metal halogen perovskite nanoparticles and metal halogen perovskite nanoparticle dispersion

机译:金属卤素钙钛矿纳米粒子的制备方法和金属卤素钙钛矿纳米粒子分散体

摘要

Provided is a method for preparing metal halide perovskite nanoparticles. Method for producing a metal halide perovskite nanoparticles of the present invention, preparing a mixed solution containing R 1 COOH, R 2 NH 2 and a solvent, the step of heat treatment after the addition of thallium (I) salt to the mixed solution And adding a metal halide (MX 2 ) solution to the heat-treated mixed solution and reacting to form TlMX 3 capped with R 1 CONHR 2 , wherein M is Sn or Pb, and X is Cl, Br or I R 1 and R 2 may be a saturated or unsaturated alkyl group having 6 to 28 carbon atoms regardless of each other. According to the present invention, by providing a method for synthesizing inorganic halogen perovskite nanoparticles using a novel stabilizer, it is possible to produce a metal alkali perovskite nanoparticles based on pseudo-alkali metal with reduced crystal defects.
机译:提供了一种制备金属卤化物钙钛矿纳米颗粒的方法。本发明的金属卤化物钙钛矿纳米颗粒的制备方法,其制备包含R 1 COOH,R 2 NH 2 和溶剂的混合溶液,将the(I)盐添加到混合溶液中,然后将金属卤化物(MX 2 )溶液添加到热处理过的混合溶液中并反应形成TlMX 3 加上R 1 CONHR 2 ,其中M为Sn或Pb,X为Cl,Br或IR 1 R 2 可以彼此独立地为碳原子数为6〜28的饱和或不饱和烷基。根据本发明,通过提供一种使用新型稳定剂合成无机卤素钙钛矿纳米颗粒的方法,可以生产基于具有减少的晶体缺陷的拟碱金属的金属碱金属钙钛矿纳米颗粒。

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