/ An reaction solution circulation type reaction system to introduce coupling agents into organic/inorganic material and a method for introducing coupling agents using the same

摘要

The present invention relates to a circulating device and method for monitoring the amount of introduction of a coupling agent in real time by controlling the amount of introduction in the organic-inorganic composite and allowing reuse of a solvent and a coupling agent used at the same time. To this end, the present invention is an initial inspection device for calculating the concentration of the reaction solution inside the reaction tank and the reaction tank for preparing the organic-inorganic complex, a separation device for separating the solution from the suspension, and an intermediate inspection device for testing the concentration of the coupling agent in the discharged solution. Includes an intermediate flow path control device that re-injects a certain amount as much as the amount used to maintain the homeostasis of the solvent concentration, a final inspection device to check the final purity and concentration of the solution, and a final flow path control device to transfer the restored solution to the reactor. To provide a reaction solution recycling system.