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APPARATUS AND METHOD FOR CRYSTALLIZING AND SUPERCRITICAL DRYING OF CULTURE FLUID

机译:结晶和超临界干燥培养液的装置和方法

摘要

An apparatus and method for crystallization and supercritical drying of a culture medium are provided. The crystallization and supercritical drying apparatus of the culture solution is an apparatus for obtaining the target material by drying a culture solution containing a first solvent and a target material dissolved in the first solvent, the high-pressure container accommodating the culture solution, the A first supply part connected to the high-pressure container to supply a second solvent to the high-pressure container, a second supply part connected to the high-pressure container to supply a third solvent to the high-pressure container, and disposed adjacent to the first supply part 1 A precooler for precooling the second solvent discharged from the supply unit, and a preheater disposed adjacent to the high-pressure container to preheat the second solvent and the third solvent supplied to the high-pressure container. The crystallization and supercritical drying method of the culture solution is a method for obtaining the target material by drying a culture solution containing a first solvent and a target material dissolved in the first solvent, wherein the first solvent is removed from the culture solution. 2, a step of crystallizing the target material by substituting with a solvent, and phase transitioning the second solvent to a supercritical phase.
机译:提供了一种用于培养基的结晶和超临界干燥的设备和方法。培养液的结晶和超临界干燥装置是通过干燥含有第一溶剂和溶解在第一溶剂中的靶材的培养液来获得靶材的装置,高压容器容纳该培养液,首先供给部连接至高压容器以向高压容器供给第二溶剂,第二供给部连接至高压容器以向高压容器供给第三溶剂,并与第一容器相邻设置供应部1用于对从供应单元排出的第二溶剂进行预冷却的预冷却器,以及与高压容器相邻布置以预热供应至高压容器的第二溶剂和第三溶剂的预热器。培养溶液的结晶和超临界干燥方法是通过干燥包含第一溶剂和溶解在第一溶剂中的靶材料的培养溶液来获得靶材料的方法,其中从培养溶液中除去第一溶剂。参照图2,通过用溶剂代替使目标材料结晶并使第二溶剂相转变为超临界相的步骤。

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