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METHOD FOR SYNTHESIS OF INTERMEDIATES USEFUL FOR PRODUCING 1,3,4-TRIAZINE DERIVATIVES
METHOD FOR SYNTHESIS OF INTERMEDIATES USEFUL FOR PRODUCING 1,3,4-TRIAZINE DERIVATIVES
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机译:合成用于生产1,3,4-三嗪衍生物的中间体的方法
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摘要
FIELD: chemical or physical processes.;SUBSTANCE: invention relates to a method of producing 1,3-diethyl-2-(2-methylhydrazinylidene)propanedioate by reacting 2-halogen-substituted diethyl malonate with methylhydrazine or a salt thereof, where the method is carried out in a solvent selected from a group consisting of alcohol, acetonitrile and any mixtures thereof, in the temperature range of 10 to 80 °C, optionally in the presence of an acid catalyst. Invention also relates to another version of the method of producing 1,3-diethyl-2-(2-methylhydrazinylidene)propanedioate.;EFFECT: disclosed is a novel method of producing 1,3-diethyl-2-(2-methylhydrazinylidene)propanedioate, which avoids undesirable hazardous oxidation and a complex side reaction.;10 cl, 4 ex
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机译:发明领域本发明涉及一种通过使2-卤素取代的丙二酸二乙酯与甲基肼或其盐反应来制备1,3-二乙基-2-(2-甲基苯二甲叉基)丙二酸酯的方法,其中该方法在选自醇,乙腈及其任何混合物的溶剂中,在10至80℃的温度范围内,任选在酸催化剂的存在下进行。本发明还涉及另一种生产1,3-二乙基-2-(2-甲基苯二甲叉基)丙二酸酯的方法。效果:公开了一种新的生产1,3-二乙基-2-(2-甲基苯二甲叉基)丙二酸酯的方法。 ,可避免有害的有害氧化和复杂的副反应。; 10 cl,4 ex
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