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Low viscosity poly-a-olefin lubricating oil and synthesis method thereof

机译:低粘度聚α-烯烃润滑油及其合成方法

摘要

The present invention provides a low viscosity poly-α-olefin lubricating oil and a synthesis method thereof. The method comprises: (1) the α-olefin raw material is subjected to dehydration treatment so that the water content in the raw material is ≤10 ppm; (2) a reaction of the dehydration treated α-olefin raw material is carried out in the presence of a complex catalyst and gaseous BF3 to obtain a reaction product, wherein the pressure of the gaseous BF3 is 0.01 to 1 MPa; (3) the reaction product obtained in step (2) is sequentially subjected to flash distillation, gas stripping, centrifugation, and washing treatment to obtain an intermediate product; (4) the intermediate product obtained in step (3) is subjected to distillation under reduced pressure to separate the unreacted α-olefin raw material and α-olefin dimers, and the remaining heavy fractions are subjected to hydrogenation saturation treatment followed by fractionation and cutting-off.
机译:本发明提供了一种低粘度的聚α-烯烃润滑油及其合成方法。该方法包括:(1)对α-烯烃原料进行脱水处理,使原料中的水分≤10ppm。 (2)将脱水处理后的α-烯烃原料在配位催化剂和BF 3气态下进行反应,得到BF 3的压力为0.01〜1MPa的反应产物。 (3)对步骤(2)中得到的反应产物依次进行闪蒸,汽提,离心和洗涤处理,得到中间产物。 (4)将步骤(3)中获得的中间产物在减压下进行蒸馏以分离未反应的α-烯烃原料和α-烯烃二聚体,并将剩余的重质馏分进行氢化饱和处理,然后进行分馏和切割。 -关。

著录项

  • 公开/公告号GB201918007D0

    专利类型

  • 公开/公告日2020-01-22

    原文格式PDF

  • 申请/专利权人 PETROCHINA COMPANY LIMITED;

    申请/专利号GB20190018007

  • 发明设计人

    申请日2019-12-09

  • 分类号

  • 国家 GB

  • 入库时间 2022-08-21 11:00:12

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