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Changes in precipitate distribution during the low-stress creep of a hydrided magnesium-zirconium alloy

机译:氢化镁锆合金低应力蠕变过程中析出物分布的变化

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Microstructural changes occurring in hydrided Mg-Zr alloy (ZR55) during creep in the stress range 1.7-9.5 MPa at temperatures between 673 and 733 K have been critically examined by optical microscopy and by scanning electron microscopy. Particular attention has been given to the distribution of precipitates with respect to the grain boundaries to elucidate the operative mechanism of deformation. Geometrical features of the formation of precipitate-denuded zones and of the concurrent accumulation of precipitates have been explored in relation to the conditions of creep and the direction of tensile stress. Additional information has been obtained from microanalysis within the grains and near grain boundaries. Clear evidence is provided that, at the lower stress levels, all such microstructural changes are consistent with those expected from a deformation mechanism controlled by diffusional flow. The measured strain rates, however, exceeded those estimated from diffusional creep theory in this alloy and the microstructural observations provide some indication of reasons for this discrepancy. [References: 35]
机译:已经通过光学显微镜和扫描电子显微镜严格检查了在1.7-9.5 MPa应力范围内在673至733 K之间的温度范围内蠕变期间,氢化Mg-Zr合金(ZR55)中发生的微观结构变化。特别注意了析出物相对于晶界的分布,以阐明变形的作用机理。相对于蠕变条件和拉伸应力的方向,已探究了析出物剥蚀区的形成和析出物同时聚集的几何特征。通过晶粒内部和晶粒边界附近的微分析获得了更多信息。提供了明确的证据,即在较低的应力水平下,所有此类微观结构变化均与由扩散流控制的变形机制所预期的变化一致。然而,所测得的应变速率超过了根据该合金的扩散蠕变理论所估计的应变速率,并且显微组织观察结果为这种差异的原因提供了一些指示。 [参考:35]

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