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首页> 外文期刊>Ceramic Engineering and Science Proceedings >THERMOPLASTIC CERAMIC INJECTION MOLDING OF ZIRCONIA TOUGHENED ALUMINA COMPONENTS
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THERMOPLASTIC CERAMIC INJECTION MOLDING OF ZIRCONIA TOUGHENED ALUMINA COMPONENTS

机译:氧化锆增韧氧化铝组分的热塑陶瓷注射成型

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摘要

Zirconia toughened alumina ceramics are interesting materials for engineering and biomedical applications due to their high strength, hardness, fracture toughness and abrasion resistance, For the same reason final machining is rather costly, making n ear net shape manufacturing technologies such as ceramic injection molding even more attractive to produce ZTA components economically. ZTA containing 10 vol-% of zirconia reinforcement of different yttria content was produced from submicron size powders. Injection molding feedstocks were prepared using a commercial binder system, homogenized at high torque. The rheological properties of the feedstocks were investigated in order to optimize the recipes and predict the molding behavior, Molded test samples - bars and plates -were produced. The debinding process was characterized by thermal analysis, the sintering process was optimized by determination of the sintering kinetics, The sintered samples in this study were characterized by SEM, bending test, hardness test and fracture toughness investigation. To clarify the transformability of zirconia, polished and grinded ZTA samples were analyzed and evaluated by X-ray diffraction, Samples had a homogeneous and defect free microstructure. The bending strength ranged between 350-700 MPa and was noticed to decline gradually as the yttria content increased. The fracture toughness varied from 5.6 to 6.2 MPa·√m at optimum sintering temperatures.
机译:氧化锆增韧氧化铝陶瓷具有很高的强度,硬度,断裂韧性和耐磨性,因此是工程和生物医学应用中令人关注的材料。出于同样的原因,最终加工的成本很高,这使得净耳形制造技术(例如陶瓷注模成型)更加昂贵。具有吸引力,可以经济地生产ZTA组件。由亚微米尺寸的粉末生产了含有10体积%的不同氧化钇含量的氧化锆增强材料的ZTA。使用商业粘合剂系统制备注射成型原料,并在高扭矩下将其均质化。为了优化配方并预测模制行为,对原料的流变特性进行了研究,生产了模制的测试样品(棒和板)。通过热分析来表征脱脂过程,通过确定烧结动力学来优化烧结过程,通过SEM,弯曲试验,硬度试验和断裂韧性研究来表征本研究中的烧结样品。为了阐明氧化锆的可转化性,对经过抛光和研磨的ZTA样品进行了分析和X射线衍射评估,样品具有均匀且无缺陷的微观结构。弯曲强度在350-700MPa之间,并且随着氧化钇含量的增加,弯曲强度逐渐下降。在最佳烧结温度下,断裂韧性为5.6〜6.2 MPa·√m。

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