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High temperature sensors fabricated on Al2O3 ceramic and nickel-based superalloy substrates

机译:在Al2O3陶瓷和镍基高温合金基底上制造的高温传感器

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The main purpose of this study is to develop resistance temperature sensors which can work at high temperature. A 2 mu m thick Al2O3 thin film was deposited as an electrical insulating film on Pt-coated Al2O3 ceramic substrates and nickel-based superalloy substrates by Dual Ion Beam Sputtering Deposition (DIBSD). The results of atomic force microscopy (AFM), scanning electron microscopy (SEM), and X-ray photon electron spectroscopy (XPS) analyses reveal that the Al2O3 films were dense, smooth and pinholes free with roughness around 3 nm. The vertical electrical resistance of thin films deposited on Pt-coated Al2O3 ceramic substrates was more than 2 G Omega at room temperature and 100 k Omega even at around 800 degrees C. Both resistance temperature sensors (RTSs) fabricated on Al2O3 ceramic substrate and that on nickel based superalloy substrates showed a linear relation up to 1000 degrees C. The RTS on the ceramic substrates showed stable after 4 thermal cycles while RTS on the superalloy substrates showed a good repeatability of heating and cooling curves even after experiencing a high temperature environment as high as 1000 degrees C. (C) 2016 Elsevier B.V. All rights reserved.
机译:这项研究的主要目的是开发可以在高温下工作的电阻温度传感器。通过双离子束溅射沉积(DIBSD)在Pt涂层的Al2O3陶瓷基板和镍基高温合金基板上沉积2 µm厚的Al2O3薄膜作为电绝缘膜。原子力显微镜(AFM),扫描电子显微镜(SEM)和X射线光子电子光谱(XPS)分析的结果表明,Al2O3薄膜致密,光滑且无针孔且粗糙度约3 nm。在室温下,沉积在涂有Pt的Al2O3陶瓷基板上的薄膜的垂直电阻大于2 G Omega,甚至在约800摄氏度时,其垂直电阻也为100k Omega。在Al2O3陶瓷基板上制造的电阻温度传感器(RTSs)和镍基高温合金基材在高达1000摄氏度的温度下显示出线性关系。陶瓷基材上的RTS在经过4个热循环后表现出稳定,而高温合金上的RTS即使经历了如此高的高温环境也显示出良好的加热和冷却曲线可重复性最高温度为1000度。(C)2016 Elsevier BV保留所有权利。

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