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Influence of compaction pressure and heating rate on tribological wear of sinters from Ti6Al4V powder manufactured by SPS

机译:压制压力和加热速率对SPS生产的Ti6Al4V粉末对烧结矿的摩擦磨损的影响

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摘要

The Ti6Al4V alloy due to its characteristics is applicable not only in technology but also in medicine, such as porous implants and solid ones. In the case of solid implants, a major problem is inadequate tribological properties of this alloy and in order to improve them, new manufacturing techniques which include the method of spark plasma sintering are applied. The article presents the preliminary tribological results of sinters from Ti6Al4V powder produced by the SPS method. Sintering using an HP D 25-3 was carried out at 1000°C over 5 min at a compaction pressure of respectively 5, 25 and 50 MPa at a heating rate of 200,300 and 400 °C/min. The resulting sinters were measured for density and hard-ness, subjected to micro structure observations and friction and wear tests using the tribological tester T-05 (block-ring tribosystem) at tribosystem load for- ces of 120, 220 and 320 N. The tests were carried out at a constant speed of 0.36 m/s on a friction path of 1000 m. The dependence of the friction coefficient changes as a function of friction path as well as specified mass and volume wear of the tested materials is presented. Observations of the bearing surface morphology of the sinters were also conducted. It was shown that the sinters fabricated at a compaction pressure of 50 MPa and heating rate of 400°C/min demonstated the least tribological wear, and the main tribological wear mechanism was abrasive wear. On the bearing surface of the tested samples there were no signs of adhesive wear.
机译:Ti6Al4V合金由于其特性而不仅适用于技术,而且还适用于医学,例如多孔植入物和固体植入物。在固体植入物的情况下,主要问题是该合金的摩擦学性能不足,并且为了改善它们,应用了包括火花等离子体烧结方法的新制造技术。本文介绍了用SPS方法生产的Ti6Al4V粉末烧结矿的初步摩擦学结果。使用HP D 25-3的烧结是在1000℃,5分钟,25和50 MPa的压实压力下,以200,300和400°C / min的加热速率进行5分钟。使用摩擦测试仪T-05(块环摩擦系统)在摩擦力为120、220和320 N的条件下,对所得的烧结体进行密度和硬度测量,并进行微观结构观察以及摩擦和磨损测试。测试在1000 m的摩擦路径上以0.36 m / s的恒定速度进行。呈现了摩擦系数随摩擦路径变化的相关性以及被测材料的指定质量和体积磨损。还观察了烧结体的轴承表面形态。结果表明,在50 MPa的压制压力和400°C / min的加热速率下制造的烧结矿显示出最小的摩擦磨损,主要的摩擦磨损机理是磨料磨损。在测试样品的轴承表面上没有粘合剂磨损的迹象。

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