Convenient synthesis of drimenol and its oxidation with selenium dioxide

K.I.Kuchkova; A.N.Aricu; I.P.Dragalin; P.F.Vlad

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Convenient synthesis of drimenol and its oxidation with selenium dioxide

机译：柠檬烯的便捷合成及其二氧化硒的氧化

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摘要

A convenient synthesis of drimenol by treatment of readily available drimane-8alpha,ll-diol 11-monoacetate with sulfuric acid in ethanol under mild conditions was developed.Oxidation of drimenol with selenium dioxide gives known drim-7-ene-9alpha,11 -diol and drim-7-ene-11,12-diol as the major products.

机译：在温和的条件下，用硫酸在乙醇中处理易得的drimane-8α，11-二醇11-单乙酸酯，从而方便地合成了drimenol.drimenol用二氧化硒氧化得到了已知的drim-7-ene-9alpha，11-diol主要产品为drim-7-ene-11,12-diol。

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《Russian Chemical Bulletin》 |2004年第12期|共4页
作者
K.I.Kuchkova; A.N.Aricu; I.P.Dragalin; P.F.Vlad;
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正文语种 eng
中图分类化学;
关键词
terpenoids; drimenol; drimane-8alpha; ll-diol 11-monoacetate; drim-7-ene-9alpha; ll-diol; drim-7-ene-ll; 12-diol; selenium dioxide; oxidation; dehydration;

机译：萜类;drimenol;drimane-8α;ll-二醇11-单乙酸酯;drim-7-ene-9alpha;ll-二醇;drim-7-ene-11;12-二醇;二氧化硒;氧化;脱水;

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1. Convenient synthesis of drimenol and its oxidation with selenium dioxide [J] . K.I.Kuchkova, A.N.Aricu, I.P.Dragalin, Russian Chemical Bulletin . 2004,第12期

机译：柠檬烯的便捷合成及其二氧化硒的氧化
2. DABCO-bis (sulfur dioxide), DABSO, as a convenient source of sulfur dioxide for organic synthesis: Utility in sulfonamide and sulfamide preparation [J] . Woolven H., González-Rodríguez C., Marco I., Organic letters . 2011,第18期

机译：DABCO-bis（二氧化硫），DABSO，作为有机合成中二氧化硫的便捷来源：用于磺酰胺和磺酰胺的制备
3. Laser desorption/ionization and laser ablation synthesis of new selenium oxide compounds from selenium(IV) dioxide [J] . Spalt Z, Pena-Mendez EM, Alberti M, Rapid Communications in Mass Spectrometry: RCM . 2006,第6期

机译：二氧化硒对新型氧化硒化合物的激光解吸/电离和激光烧蚀合成
4. Alternating Copolymerization of Carbon Dioxide and Epoxide. The First Example of Polycarbonate Synthesis from 1-atm Carbon Dioxide by Manganese Porphyrin [C] . International Conference on Carbon Dioxide Utilization . 2004

机译：交替的二氧化碳和环氧化物共聚。通过锰卟啉从1 atm二氧化碳聚碳酸酯合成的第一个例子
5. I. Oxidation-Initiated Nazarov Cyclization of Vinyl Alkoxyallenes. II. Efforts Toward an Improved Synthesis of Rocaglamide Amenable to Analog Synthesis. III. A Convenient Cycloaromatization Protocol for Synthesis of Polysubstituted Phenol Derivatives: Method Development and Mechanistic Studies [D] . Spencer, William T., III 2013

机译：I.乙烯基烷氧基丙烯烯的氧化引发的纳扎罗夫环化。二。努力进行适于模拟合成的罗卡酰胺的合成。三，合成多取代苯酚衍生物的便捷环芳构化方法：方法开发和机理研究
6. Solvent‐Dependent Facile Synthesis of Diaryl Selenides and Biphenols Employing Selenium Dioxide [O] . Thomas Quell, Dr. Michael Mirion, Dr. Dieter Schollmeyer, 2016

机译：使用二氧化硒的溶剂依赖性二芳基硒化物和双酚的简便合成
7. Hydrogen Peroxide Oxidation. I. A New Selenium Dioxide-Catalyzed Synthesis of Carboxylic Acids from Aliphatic Ketones Accompanied by Rearrangement of Alkyl Groups [O] . Noboru Sonoda, Shigeru Tsutsumi 1959

机译：过氧化氢氧化。 I.来自脂酮酮的新硒催化合成羧酸的羧酸伴随烷基的重排
8. Reactions of Bis(pentafluoroselenium) Peroxide: Synthesis of Pentafluoroselenium Fluorosulfate and of Bis(pentafluoroselenium) Oxide [R] . Reichert, W. L., Cady, G. H. 1972

机译：双（五氟硒）过氧化物的反应：五氟硒氟硫酸盐和双（五氟硒）氧化物的合成

Convenient synthesis of drimenol and its oxidation with selenium dioxide

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