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Cutting Cost Technology for the Preparation of Biodiesel Using Environmentally Benign and Cheaper Catalyst

机译:使用环境友好且廉价的催化剂制备生物柴油的低成本技术

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摘要

Herein, a promising egg shell derived catalyst (ESDC) was prosperously developed by calcination of egg shell powder and exercised to the transesterification of Helianthus annuus L oil for the synthesis of biodiesel fuel. Synthesized egg shell derived catalyst affirmed remarkable catalytic activity for transesterification of Helianthus annuus L oil with 2.5 % catalyst dose (w/w). ESDC was duly characterized by FT-IR, XRD, BET, TPD-CO2, TGA and SEM analysis. While, Helianthus annuus L oil and biodiesel were duly characterized by FT-IR as well as H-1 and C-13 NMR spectroscopic techniques. From the obtained results, it can be concluded that 1:8 oil to methanol molar ratio revealed 99.2 % biodiesel yield in 2 h reaction time with 2.5 % catalyst dosage at 65 A degrees C reaction temperature.
机译:本文中,通过煅烧蛋壳粉而繁荣地开发了有前途的蛋壳衍生催化剂(ESDC),并将其用于向日葵油的酯交换反应以合成生物柴油燃料。合成的蛋壳衍生催化剂证实了在2.5%催化剂剂量(w / w)下对向日葵油进行酯交换反应具有显着的催化活性。通过FT-IR,XRD,BET,TPD-CO2,TGA和SEM分析对ESDC进行了适当的表征。同时,通过FT-IR以及H-1和C-13 NMR光谱技术对向日葵油和生物柴油进行了适当表征。从获得的结果可以得出结论,油与甲醇的摩尔比为1:8,在65°C的反应温度下2小时的反应时间内,以2.5%的催化剂用量,生物柴油产率为99.2%。

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