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Wear studies on ZrO2-filled PEEK as coating bearing materials for artificial cervical discs of Ti6Al4V

机译:ZrO2填充的PEEK作为Ti6Al4V人造颈椎间盘的涂层轴承材料的磨损研究

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摘要

Polyetheretherketone (PEEK) and its composite coatings are believed to be the potential candidates' bio-implant materials. However, these coatings have not yet been used on the surface of titanium-based orthopedics and joint products and very few investigations on the tribological characteristics could be found in the published literature till date. In this study, the wettabilities, composition and micro-hardness were characterized using contact angle measurement, scanning electron microscopy (SEM) and hardness tester. The tribological tests were conducted using a ball-on-disc contact pair under 25% newborn calf serum (NCS) lubricated condition. For comparison, bare Ti6Al4V was studied. The obtained results revealed that those PEEK/ZrO2 composite coatings could improve the tribological properties of Ti6Al4V significantly. Adhesive wear and mild abrasive wear might be the dominant wear and failure mechanisms for PEEK/ZrO2 composite coatings in NCS lubricated condition. After comprehensive evaluation in the present study, 5 wt.% ZrO2 nanoparticles filled PEEK coating displayed the optimum tribological characteristics and could be taken as a potential candidate for the bearing material of artificial cervical disc (C) 2016 Elsevier B.V. All rights reserved.
机译:聚醚醚酮(PEEK)及其复合涂层被认为是潜在的候选生物植入材料。但是,这些涂层尚未在钛基骨科和关节产品的表面上使用,到目前为止,在摩擦学特性方面的研究很少见。在这项研究中,使用接触角测量,扫描电子显微镜(SEM)和硬度测试仪来表征润湿性,组成和显微硬度。在25%新生小牛血清(NCS)润滑条件下,使用圆盘接触对进行摩擦学测试。为了比较,研究了裸Ti6Al4V。所得结果表明,这些PEEK / ZrO2复合涂层可以显着改善Ti6Al4V的摩擦学性能。在NCS润滑条件下,PEEK / ZrO2复合涂层的粘着磨损和轻度磨料磨损可能是主要的磨损和失效机理。经过本研究的综合评估后,填充PEEK涂层的5 wt。%ZrO2纳米颗粒表现出最佳的摩擦学特性,可以作为人造颈椎间盘(C)2016 Elsevier B.V.轴承材料的潜在候选者。保留所有权利。

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