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Multiform structures of SnO2 nanobelts

机译:SnO2纳米带的多种结构

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摘要

Multiform SnO2 microstructures were synthesized by a facile thermal evaporation of tin grains. The product was characterized with a variety of techniques to obtain the structural and optical information. Scanning electron microscopy ( SEM) and transmission electron microscopy ( TEM) images showed a large percentage of acute angle zigzag nanobelts with perfectly periodic morphology. High resolution transmission electron microscopy ( HRTEM) images and selected area electron diffraction ( SAED) patterns revealed that the zigzag nanobelts were single crystalline and their zone axis was along the [ 010] crystal direction. The growth mechanism of zigzag nanobelts was proposed based on TEM characterization and thermodynamic analysis. The zigzag nanobelts were deduced to be formed by changing the growth direction from [ 101] to [ 101] or vice versa. The photoluminescence ( PL) spectroscopy of the nanobelts showed a broad and strong luminescence emission centred at 550 nm.
机译:通过锡晶粒的快速热蒸发合成了多种形式的SnO2微观结构。用多种技术对产品进行表征,以获得结构和光学信息。扫描电子显微镜(SEM)和透射电子显微镜(TEM)图像显示,锐角之字形纳米带中有很大一部分具有完美的周期性形态。高分辨率透射电子显微镜(HRTEM)图像和选定区域电子衍射(SAED)模式显示,之字形纳米带是单晶的,其带区轴沿[010]晶体方向。基于TEM表征和热力学分析,提出了曲折形纳米带的生长机理。通过将生长方向从[101]更改为[101],反之亦然可以推断出之字形纳米带。纳米带的光致发光(PL)光谱显示了以550 nm为中心的宽而强的发光发射。

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