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Analytical study of fundamental nanoindentation test relations for indenters of non-ideal shapes

机译:非理想形状压头的基本纳米压痕测试关系的分析研究

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Nanoindentation techniques provide a unique opportunity to obtain mechanical properties of materials of very small volumes. The load-displacement and load-area curves are the basis for nanoindentation tests, and their interpretation is usually based on the main assumptions of the Hertz contact theory and formulae obtained for ideally shaped indenters. However, real indenters have some deviation from their nominal shapes leading researchers to develop empirical 'area functions' to relate the apparent contact area to depth. We argue that for both axisymmetric and three-dimensional cases, the indenter shape near the tip can be well approximated by monomial functions of radius. In this case problems obey the self-similar laws. Using Borodich's similarity considerations of three-dimensional contact problems and the corresponding formulae, fundamental relations are derived for depth of indentation, size of the contact region, load, hardness, and contact area, which are valid for both elastic and non-elastic, isotropic and anisotropic materials. For loading the formulae depend on the material hardening exponent and the degree of the monomial function of the shape. These formulae are especially important for shallow indentation (usually less than 100 nm) where the tip bluntness is of the same order as the indentation depth. Uncertainties in nanoindentation measurements that arise from geometric deviation of the indenter tip from its nominal geometry are explained and quantitatively described.
机译:纳米压痕技术提供了获得极小体积材料机械性能的独特机会。载荷-位移和载荷-面积曲线是纳米压痕测试的基础,它们的解释通常基于赫兹接触理论的主要假设以及理想形状的压头获得的公式。但是,真正的压头与其名义形状有些偏差,导致研究人员开发出经验“面积函数”以将表观接触面积与深度联系起来。我们认为,对于轴对称和三维情况,尖端附近的压头形状都可以通过半径的单项函数很好地近似。在这种情况下,问题遵循自相似定律。使用三维接触问题的Borodich相似性考虑因素和相应的公式,得出压痕深度,接触区域的大小,载荷,硬度和接触面积的基本关系,这些关系对于弹性和非弹性均质均有效和各向异性材料。对于加载,公式取决于材料的硬化指数和形状的单项函数的程度。这些公式对于浅压痕(通常小于100 nm)尤其重要,在浅压痕中,尖端钝度与压痕深度相同。纳米压痕测量的不确定性是由压头尖端与其标称几何形状的几何偏差引起的,并对此进行了定量描述。

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