A new synthesis of a nitroimino-containing 1,2,4-triazin-5-one from 3-bromo-3-nitropropenoates

Berestovitskaya Valentina M.; Ozerova Olga Yu.; Efimova Tatiana P.; Gurzhiy Vladislav V.; Novikova Tamara A.

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A new synthesis of a nitroimino-containing 1,2,4-triazin-5-one from 3-bromo-3-nitropropenoates

机译：由3-溴-3-硝基丙酸酯合成含硝基亚氨基的1,2,4-三嗪-5-酮

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摘要

Reaction of 1-amino-2-nitroguanidine with alkyl 3-bromo-3-nitropropenoates affords 3-nitrohnino-6-nitromethyl-4,5-dihydro-(2H)-1,2,4-triazin-5-one, whose structure was characterized by IR, UV, NMR spectroscopy and X-ray single crystal analysis.

机译：1-氨基-2-硝基胍与3-溴-3-硝基丙酸烷基酯的反应，得到3-硝基氨基-6-硝基甲基-4,5-二氢-（（2H）-1,2,4-三嗪-5-酮通过IR，UV，NMR光谱和X射线单晶分析表征其结构。

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《Mendeleev Communications 》 |2016年第4期| 共3页
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Berestovitskaya Valentina M.; Ozerova Olga Yu.; Efimova Tatiana P.; Gurzhiy Vladislav V.; Novikova Tamara A.;
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1. A new synthesis of a nitroimino-containing 1,2,4-triazin-5-one from 3-bromo-3-nitropropenoates [J] . Berestovitskaya Valentina M., Ozerova Olga Yu., Efimova Tatiana P., Mendeleev Communications . 2016 ,第4期

机译：由3-溴-3-硝基丙酸酯合成含硝基亚氨基的1,2,4-三嗪-5-酮
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机译：氟化杂环化合物。通过3-苯甲酰-5-全氟烷基 - 烯型反应合成3-全氟烷基-6-苯基-2H-1,2,4-三嗪-5-苯基-2H-1,2,4-三嗪-5- 5-氟化氟聚酯的有效策略1,2,4-氧代唑和肼。

A new synthesis of a nitroimino-containing 1,2,4-triazin-5-one from 3-bromo-3-nitropropenoates

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