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Electron‐beam‐induced current and TEM studies of stacking faults formed by the oxidation of boron‐implanted silicon

机译:硼氧化形成的硼连字符;注入硅形成的堆叠故障的电子连字符连字符连字符;感应电流和TEM研究

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The electron‐beam‐induced conductivity (EBIC) of emitter‐base junctions was studied in a scanning electron microscope, and the image contrast of process‐induced stacking faults was investigated by transmission electron microscopy (TEM). Emitter‐base (e‐b) junctions were formed by phosphorus diffusion into boron‐implanted bases on ⟨100⟩ silicon. The implanted bases were preannealed in an oxidizing atmosphere, which generates stacking faults. The e‐b junctions were designed with metal contacts removed such that the active e‐b region was ’’open’’ to EBIC analysis. Leaky junctions (i.e., 104nA/cm2) were found when relatively high concentrations of oxygen were used in the annealing atmosphere (e.g., 10 O2). These junctions exhibited a mottled contrast in the EBIC mode, indicative of a high density of recombination centers. Relatively low‐leakage junctions (i.e., 10 nA/cm2) were found when a 1‐O2atmosphere was used and the junctions contained an occasional stacking fault. These stacking faults exhibited an EBIC contrast characteristic of recombination at partial dislocations bounding the faults. Diffraction‐contrast experiments using TEM showed that isolated stacking faults in the base region were extrinsic in nature and were not decorated by heavy metal microprecipitates. The generation currents for ’’clean’’ extrinsic stacking faults were estimated to be in the range 10−2–10−4nA per stacking fault for these junctions.
机译:在扫描电子显微镜下研究了发射极&连字符-基极结的电子&连字符&连字符&诱导电导率(EBIC),并利用透射电子显微镜(TEM)研究了过程&连字符诱导堆叠故障的图像对比度.发射极&连字符;碱(e&连字符;b)结是通过磷扩散到〈100〉硅上的硼&连字符;注入的碱基形成的。植入的碱在氧化气氛中进行预退火,这会产生堆叠故障。e‐b结的设计去除了金属触点,使得有源的e&hyph;b区域对EBIC分析是“开放的”。当在退火气氛中使用相对较高浓度的氧气(例如,10% O2)时,发现泄漏结(即104nA/cm2)。这些结在EBIC模式下表现出斑驳的对比度,表明复合中心的密度很高。当使用1%‐O2大气压时,发现泄漏结相对较低(即10 nA/cm2),并且这些结中偶尔存在堆积故障。这些堆积断层在断层边界的部分位错处表现出复合的EBIC对比特征。透射电镜衍射对比实验表明,基区孤立的堆积断层本质上是外在的,没有被重金属微沉淀物修饰。据估计,这些结点的每个堆叠断层的“干净”外部堆积断层的产生电流在10-2-10-4nA的范围内。

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