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In_2O_3 nanofibers and nanoribbons: Preparation by electrospinning and their formaldehyde gas-sensing properties

机译:In_2O_3纳米纤维和纳米带:静电纺丝制备及其对甲醛的气敏特性

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摘要

In_2O_3 nanofibers and nanoribbons were prepared by electrospinning combined with a polyvinyl pyrrolidone)-assisted sol-gel technique. By tuning the experimental parameters, the morphological transformation of In_2O_3 from nanofibers to nanoribbons was achieved. It was found that both the rapid evaporation of solvent and the concentration of the precursor played important roles in the formation process of In_2O_3 nanoribbons. The average diameter of the In _2O_3 nanofibers is 180 nm. The nanoribbons have an average width of 1 μn and a thickness of about 150 nm. The lengths of both can reach millimeters. The average grain size consisting of nanofibers and nanoribbons is 18.6 and 11.2 nm, respectively. The gas-sensing properties of In _2O_3 nanofibers and nanoribbons toward formaldehyde vapor were investigated. Interestingly, the gas sensor fabricated with In _2O_3 nanoribbons exhibited a higher and faster response at a relatively lower operating temperature than that fabricated with nanofibers.
机译:In_2O_3纳米纤维和纳米带是通过电纺结合聚乙烯吡咯烷酮辅助溶胶-凝胶技术制备的。通过调整实验参数,实现了In_2O_3从纳米纤维到纳米带的形态转变。发现溶剂的快速蒸发和前体的浓度在In_2O_3纳米带的形成过程中都起着重要作用。 In _2O_3纳米纤维的平均直径为180 nm。纳米带具有1μn的平均宽度和约150nm的厚度。两者的长度都可以达到毫米。由纳米纤维和纳米带组成的平均晶粒尺寸分别为18.6和11.2 nm。研究了In _2O_3纳米纤维和纳米带对甲醛蒸气的气敏特性。有趣的是,与用纳米纤维制成的气体传感器相比,用In _2O_3纳米带制成的气体传感器在相对较低的工作温度下表现出更高且更快的响应。

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