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Hot utility of aluminium and titanium containing steels with and without cyclic temperature oscillations

机译:含和不含循环温度波动的含铝和钛钢的热应用

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摘要

The hot ductility of alow and high Al containing steel having 0.1 percent C and 0.4 percent Mn has been examined. The steels were heated to 1350 deg C and then cooled to test temperatures in the range 1000-700 deg C at 60 K min~(-1) and strained to failure at a strain rate of 10~(-3) s~(-1). The effects on hot ductility of undercooling by 100 K before testing and giving a full single cycle with an amplitude of 100 K were also determined. Cooling directly to the test temperature gave a hot ductility trough for the low Al containing steel which spanned the temperature range from the Ae_3to the Ar_3 (undf formed). Failure in the trough was intergranular ductile due to microvoid coalescence at MnS inclusions situated in the softer deformation induced ferrite phase surrounding the y grains. Ductility was good at temperatures above the Ae_3 because of dynamic recrystallisation and good below the Ar_3as large amounts of ferrite formed before deformation. Increasing the Al content extended the trough to higher temperatures due to precipitation of AIN which encouraged grain boundary sliding and delayed the onset of dynamic recrystallisation. Undercooling by 100 K caused ferrite to be introduced before testing for temperatures below the Ar_3, and this remained on reheating to the test temperature. The undercooling in the y range also encouraged precipitation of AIN which increased the temperature for the onset of dynamic recrystallisation. The troughs were consequently raised by 50-100 K. The single cycle caused additional AIN to be precipitated resulting in an extension of the trough for the low Al containing steel, but not in the high Al steel, since its ductility had already been seriously impaired by marked AIN precipitation. A Ti containing steel with a high Al content and a higher Mn steel with low Al content were also studied, but without undercooling or cycling. The Ti containing steel gave a very narrow trough due to (i) removal of N so that AIN could not form and (ii) a finer grain size owing to the presence of TiN particles. The finer grain size reduced the depth of the trough but also encouraged deformation induced ferrite to form so that ductility recovered at temperatures close to the Ae_3. Increasing the Mn content shifted the trough to lower temperatures in accordance with the steels' lower transformation temperatures and gave a shallower trough due to reduced precipitation of the finer MnS inclusions at the gamma grain boundaries.
机译:已经研究了具有0.1%C和0.4%Mn的低铝和高铝钢的热延展性。将钢加热到1350摄氏度,然后在60 K min〜(-1)下冷却至1000-700℃的测试温度,并以10〜(-3)s〜(-的应变速率应变至失效。 1)。还确定了在测试之前过冷100 K并给出幅度为100 K的完整单循环对过冷性的热延展性的影响。直接冷却到测试温度为低铝含量的钢提供了一个热延展性低谷,其温度范围从Ae_3到Ar_3(形成无定形)。由于在y晶粒周围较软的变形引起的铁素体相中的MnS夹杂物的微空隙聚结,槽中的破坏是晶间延性的。由于动态再结晶,在高于Ae_3的温度下,延展性良好;而在变形之前形成大量铁素体,则在Ar_3以下的延展性良好。由于AIN的沉淀,增加Al的含量将槽延伸到更高的温度,这促进了晶界滑动并延迟了动态再结晶的开始。在测试低于Ar_3的温度之前,过冷100 K会导致引入铁氧体,并且在重新加热至测试温度时仍然存在。 y范围内的过冷也促进了AIN的沉淀,这增加了动态重结晶开始的温度。槽因此升高了50-100K。单周期导致额外的AIN析出,导致含铝量低的钢的槽扩展,但含铝量高的钢却没有,因为其延展性已经严重受损。通过明显的AIN沉淀。还研究了含铝量高的含钛钢和含铝量低的高锰钢,但没有过冷或循环。含Ti的钢槽非常狭窄,这是由于(i)去除了N,所以不能形成AIN,以及(ii)由于存在TiN颗粒而使晶粒尺寸更细。较细的晶粒尺寸减小了槽的深度,但也促进了变形引起的铁素体的形成,从而在接近Ae_3的温度下恢复了延展性。 Mn含量的增加会根据钢的较低相变温度将槽移至较低的温度,并且由于减少了较细的MnS夹杂物在γ晶界处的析出而使槽较浅。

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