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Microstructural stability and creep behavior of a lamellar gamma-TiAl based alloy with extremely fine lamellar spacing

机译:具有极细层间距的层状γ-TiAl基合金的组织稳定性和蠕变行为

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Lamellar Ti-46Al-1.5Cr-2Mo-0.25Si-0.3B (in at. percent) specimens with two different extremely fine lamellar spacings were produced and investigated. The average lamellar spacing was determined to be 200 and 35 nm, respectively. Creep tests at 700 deg C have shown a distinct primary creep regime for both material conditions. After annealing for 24h at 1000 deg C the primary creep strain for both materials is significantly decreased. The steady-state creep for the specimens with the wider lamellar spacing appears to be similar to the creep behavior prior to annealing while the creep rate of the material with the previously smaller lamellar spacing is significantly higher. Optical microscopy and TEM-studies show that the microstructure of the specimens with the wider lamellar spacing is nearly unchanged, whereas the previously finer material was completely recrystallized to an equiaxed gamma microstructure with a low creep resistance. The dissolution of the fine lamellar microstructure was also observed during creep tests at 800 deg C as manifested in an acceleration of the creep rate.
机译:制作并研究了具有两个不同的极细薄片间距的薄片Ti-46Al-1.5Cr-2Mo-0.25Si-0.3B(原子百分比)样品。测得的平均层间距分别为200和35 nm。在700摄氏度下的蠕变测试表明,两种材料条件下都有明显的初始蠕变状态。在1000摄氏度下退火24小时后,两种材料的初始蠕变应变均显着降低。具有较宽层状间距的样品的稳态蠕变似乎与退火之前的蠕变行为相似,而具有先前较小层状间距的材料的蠕变速率则明显更高。光学显微镜和TEM研究表明,具有较宽层状间距的试样的微观结构几乎未变,而先前较细的材料已完全重结晶为具有低抗蠕变性的等轴γ微观结构。在蠕变速率的加速中可以看出,在800摄氏度的蠕变测试过程中还观察到了精细的层状微结构的溶解。

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