Synthesis and Crystal Structure of Diethyl Dithiocarbamate Tellurium

摘要

Diethyl dithiocarbamate tellurium was synthesized and characterized by ER spectra,elemental analysis,and single-crystal X-ray diffraction analysis.The crystal structure of tellurium complex was determined by single-crystal X-ray.The possessing parameters:P2(1)/c,a=15.1640(3)A,b=8.4055(2)A,c=14.7887(2)A,alpha=90°,beta=117.228(10)°,gamma=90°,V=1676.1(6)A~3,Z=4,Mr=424.12,Dc=1.681 g/cm~3,mu=2.256 mm~(-1),F(000)=840,T=296(2)K,R1=0.0246,wR2=0.0603 for 3799 reflections with I > 2 sigma(I).