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Investigating the Catalytic Performance of Graphene Oxide -Polyaniline -Lignosulfonate Nanocomposite in the Synthesis of Polysubstituted Pyridines via a Four-Component Reaction

机译:研究石墨烯 - 氧化石墨烯 - 聚烷氨基磺酸盐纳米复合材料的催化性能通过四组分反应合成多硫酸吡啶。

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摘要

In this research, graphene oxide -polyaniline-lignosulfonate (GO-PANI-LS) nanocomposite was synthesized successfully and it was used as an effective recyclable catalyst for the synthesis of polysubstituted pyridines. Characterization of the prepared nanocomposite was carried out by Fourier transform infrared radiation (FT-IR), X-ray diffraction patterns (XRD), Energy-dispersive x-ray spectroscopy (EDX), Field-emission scanning electron microscopy (FE-SEM) and Thermogravimetric analysis (TGA). The first report of using this nanocomposite as a heterogeneous catalyst in synthesis of polysubstituted pyridines, Eco-friendly, high catalytic activity of catalyst, simplicity of procedure, mild reaction conditions, easy recovery and considerable reusability without significant loss of performance are advantages of this method.
机译:在这项研究中,成功合成了氧化石墨烯 - 多聚烷氨二磺酸盐(GO-PANI-LS)纳米复合材料,并用作合成多求二取代吡啶的有效可回收催化剂。 通过傅立叶变换红外辐射(FT-IR),X射线衍射模式(XRD),能量分散性X射线光谱(EDX),现场发射扫描电子显微镜(FE-SEM)来进行制备的纳米复合材料的表征。 和热重分析(TGA)。 首次使用该纳米复合材料作为综合吡啶,生态友好,催化剂的高催化活性,程序简单,轻度反应条件,易于恢复和相当大的可重复性而无需大量绩效的优势的首次报道 。

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