首页> 外文期刊>Rapid Communications in Mass Spectrometry: RCM >Coupling trapped ion mobility spectrometry to mass spectrometry: trapped ion mobility spectrometry–time‐of‐flight mass spectrometry versus trapped ion mobility spectrometry–Fourier transform ion cyclotron resonance mass spectrometry

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Coupling trapped ion mobility spectrometry to mass spectrometry: trapped ion mobility spectrometry–time‐of‐flight mass spectrometry versus trapped ion mobility spectrometry–Fourier transform ion cyclotron resonance mass spectrometry

机译：耦合捕获的离子迁移谱法质谱法：捕获离子迁移光谱 - 飞行时间的飞行时间质谱法与捕获离子迁移光谱 - 傅里叶变换离子回旋谐振质谱法

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Rationale >There is a need for fast, post‐ionization separation during the analysis of complex mixtures. In this study, we evaluate the use of a high‐resolution mobility analyzer with high‐resolution and ultrahigh‐resolution mass spectrometry for unsupervised molecular feature detection. Goals include the study of the reproducibility of trapped ion mobility spectrometry (TIMS) across platforms, applicability range, and potential challenges during routine analysis. </section> <section xml:id="rcm8165-sec-0002" numbered="no"> <title type="main">Methods > A TIMS analyzer was coupled to time‐of‐flight mass spectrometry (TOF MS) and Fourier transform ion cyclotron resonance mass spectrometry (FT‐ICR MS) instruments for the analysis of singly charged species in the m / z 150–800 range of a complex mixture (Suwannee River Fulvic Acid Standard). Molecular features were detected using an unsupervised algorithm based on chemical formula and IMS profiles. </section> <section xml:id="rcm8165-sec-0003" numbered="no"> <title type="main">Results > TIMS‐TOF MS and TIMS‐FT‐ICR MS analysis provided 4950 and 7760? m / z signals, 1430 and 3050 formulas using the general C <sub> x </sub> H <sub> y </sub> N <sub>0–3</sub> O <sub>0–19</sub> S <sub>0–1</sub> composition, and 7600 and 22 350 [ m / z ; chemical formula; K; CCS] featu </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span>None </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-26627/'>《Rapid Communications in Mass Spectrometry: RCM》</a> <b style="margin: 0 2px;">|</b><span>2018年第15期</span><b style="margin: 0 2px;">|</b><span>共9页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Tose Lilian V.&option=202" target="_blank" rel="nofollow">Tose Lilian V.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Benigni Paolo&option=202" target="_blank" rel="nofollow">Benigni Paolo;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Leyva Dennys&option=202" target="_blank" rel="nofollow">Leyva Dennys;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Sundberg Abigail&option=202" target="_blank" rel="nofollow">Sundberg Abigail;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ramírez César E.&option=202" target="_blank" rel="nofollow">Ramírez César E.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ridgeway Mark E.&option=202" target="_blank" rel="nofollow">Ridgeway Mark E.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Park Melvin A.&option=202" target="_blank" rel="nofollow">Park Melvin A.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Rom?o Wanderson&option=202" target="_blank" rel="nofollow">Rom?o Wanderson;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Jaffé Rudolf&option=202" target="_blank" rel="nofollow">Jaffé Rudolf;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Fernandez‐Lima Francisco&option=202" target="_blank" rel="nofollow">Fernandez‐Lima Francisco;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Petroleomic and Forensic Chemistry Laboratory Department of ChemistryFederal University of Espírito Santo29075‐910 Vitória ES Brazil;</p> <p>Department of Chemistry and BiochemistryFlorida International UniversityMiami FL 33199 USA;</p> <p>Department of Chemistry and BiochemistryFlorida International UniversityMiami FL 33199 USA;</p> <p>Department of Chemistry and BiochemistryFlorida International UniversityMiami FL 33199 USA;</p> <p>Department of Chemistry and BiochemistryFlorida International UniversityMiami FL 33199 USA;</p> <p>Bruker Daltonics Inc.Billerica MA 01821 USA;</p> <p>Bruker Daltonics Inc.Billerica MA 01821 USA;</p> <p>Petroleomic and Forensic Chemistry Laboratory Department of ChemistryFederal University of Espírito Santo29075‐910 Vitória ES Brazil;</p> <p>Department of Chemistry and BiochemistryFlorida International UniversityMiami FL 33199 USA;</p> <p>Department of Chemistry and BiochemistryFlorida International UniversityMiami FL 33199 USA;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1187.html" title="分析化学">分析化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> </p> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a 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E.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Bruce, J. E.,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext= Eyler, J. R.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> Eyler, J. R. </a> <span>1992</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：通过离子 - 分子反应动力学探测捕获的离子能量：傅里叶变换离子回旋共振质谱。</span> </p> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-66778_thesis/020223011486.html">In vitro/in vivo metabolism of ginsenoside Rg5 in rat using ultra-performance liquid chromatography/quadrupole-time-of-flight mass spectrometry</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Chao Hong&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . Chao Hong</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ping Yang&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,Ping Yang</a> <span> <a href="/conference-cn-66778/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 世界中医药大会第四届夏季峰会暨世界中医药学会体质研究专业委员会第七届学术年会 </a> <span> <span> . 2018</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06130415320025.html">Fourier transform ion cyclotron resonance mass spectrometer and method for concentrating ions for fourier transform ion cyclotron resonance mass spectrometry</a> <b>[P]</b> . <span> 外国专利：  US9129784B2 </span> <span> . 2015-09-08</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：傅立叶变换离子回旋共振质谱仪和富集离子的方法 </span> </p> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06130420822884.html">FOURIER TRANSFORM ION CYCLOTRON RESONANCE MASS SPECTROMETER AND METHOD FOR CONCENTRATING IONS FOR FOURIER TRANSFORM ION CYCLOTRON RESONANCE MASS SPECTROMETRY</a> <b>[P]</b> . <span> 外国专利：  US2013228681A1 </span> <span> . 2013-09-05</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：傅立叶变换离子回旋共振质谱仪和富勒森变换离子回旋共振质谱仪中离子的浓缩方法 </span> </p> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130419368166.html">FOURIER TRANSFORM ION CYCLOTRON RESONANCE MASS SPECTROMETER AND METHOD FOR CONCENTRATING IONS FOR FOURIER TRANSFORM ION CYCLOTRON RESONANCE MASS SPECTROMETRY</a> <b>[P]</b> . <span> 外国专利：  KR101239747B1 </span> <span> . 2013-03-06</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：傅立叶变换离子回旋共振质谱仪和富勒森变换离子回旋共振质谱仪中离子的浓缩方法 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704028895609','4',7,2,1,'',this,24)" class="delivery" prompt="010401" title="通过人工服务将文献原文发送至邮箱" >获取原文</div> <div class="journalsub-pop-up" style="display: none"> <div class="journal-sub"> <h2>期刊订阅</h2> <img src="https://cdn.zhangqiaokeyan.com/img/loginclose.png" alt="" onclick="$('.journalsub-pop-up').hide()"> <p class="pardon">抱歉，该期刊暂不可订阅，敬请期待！</p> <p class="current">目前支持订阅全部北京大学中文核心（2020）期刊目录。</p> <div style="display: flex;margin-top: 69px;justify-content: space-between;"> <div 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