首页> 外文期刊>Rapid Communications in Mass Spectrometry: RCM >Coupling trapped ion mobility spectrometry to mass spectrometry: trapped ion mobility spectrometry–time‐of‐flight mass spectrometry versus trapped ion mobility spectrometry–Fourier transform ion cyclotron resonance mass spectrometry

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Coupling trapped ion mobility spectrometry to mass spectrometry: trapped ion mobility spectrometry–time‐of‐flight mass spectrometry versus trapped ion mobility spectrometry–Fourier transform ion cyclotron resonance mass spectrometry

机译：耦合捕获的离子迁移谱法质谱法：捕获离子迁移光谱 - 飞行时间的飞行时间质谱法与捕获离子迁移光谱 - 傅里叶变换离子回旋谐振质谱法

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Rationale >There is a need for fast, post‐ionization separation during the analysis of complex mixtures. In this study, we evaluate the use of a high‐resolution mobility analyzer with high‐resolution and ultrahigh‐resolution mass spectrometry for unsupervised molecular feature detection. Goals include the study of the reproducibility of trapped ion mobility spectrometry (TIMS) across platforms, applicability range, and potential challenges during routine analysis. </section> <section xml:id="rcm8165-sec-0002" numbered="no"> <title type="main">Methods > A TIMS analyzer was coupled to time‐of‐flight mass spectrometry (TOF MS) and Fourier transform ion cyclotron resonance mass spectrometry (FT‐ICR MS) instruments for the analysis of singly charged species in the m / z 150–800 range of a complex mixture (Suwannee River Fulvic Acid Standard). Molecular features were detected using an unsupervised algorithm based on chemical formula and IMS profiles. </section> <section xml:id="rcm8165-sec-0003" numbered="no"> <title type="main">Results > TIMS‐TOF MS and TIMS‐FT‐ICR MS analysis provided 4950 and 7760? m / z signals, 1430 and 3050 formulas using the general C <sub> x </sub> H <sub> y </sub> N <sub>0–3</sub> O <sub>0–19</sub> S <sub>0–1</sub> composition, and 7600 and 22 350 [ m / z ; chemical formula; K; CCS] featu </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract XMLNS =“http://www.wiley.com/namespaces/wiley”type =“main”xml：lang =“en”> <section xml：id =“rcm8165-sec-0001”编号=“否” > <标题类型=“main”>基本原理</ title> >需要快速，电离后分离在复杂混合物的分析过程中。在这项研究中，我们评估了高分辨率移动分析仪的使用，具有用于无监督的分子特征检测的高分辨率和超高分辨率质谱。目标包括在常规分析期间跨平台，适用性范围和潜在挑战的捕获离子迁移光谱（TIMS）的再现性的研究。</ p> </ section> <section XML：ID =“RCM8165-SEC-0002”编号=“否”> <标题类型=“main”>方法</ title> > TIMS分析器耦合到飞行时间质谱（TOF MS）和傅里叶变换离子回旋谐振质谱（FT-ICR MS）用于分析单独带电物种的仪器在 m型/ 150-800范围内的复合物混合物（Suwannee河富含酸标准）中。使用基于化学式和IMS型材的无监督算法检测分子特征。 </ p> </ section> <section XML：ID =“RCM8165-SEC-0003”编号=“否”> <标题类型=“main”>结果</ title> > TIMS-TOF MS和TIMS- FT-ICR MS分析提供4950和7760？使用通用C <sub> x </ sum> h <sub> x / i>信号，1430和3050配方，1430和3050配方</ i> </ sub> n <sub> 0-3 </ sub> O <sub> 0-19 </ sub> s <sub> 0-1 </ sub>组成，7600和22 350 [< i> m </ i> / z </ i>;化学式; k; CCS]专辑 </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-26627/'>《Rapid Communications in Mass Spectrometry: RCM》</a> <b style="margin: 0 2px;">|</b><span>2018年第15期</span><b style="margin: 0 2px;">|</b><span>共9页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Tose Lilian V.&option=202" target="_blank" rel="nofollow">Tose Lilian V.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Benigni Paolo&option=202" target="_blank" rel="nofollow">Benigni Paolo;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Leyva Dennys&option=202" target="_blank" rel="nofollow">Leyva Dennys;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Sundberg Abigail&option=202" target="_blank" rel="nofollow">Sundberg Abigail;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ramírez César E.&option=202" target="_blank" rel="nofollow">Ramírez César E.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ridgeway Mark E.&option=202" target="_blank" rel="nofollow">Ridgeway Mark E.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Park Melvin A.&option=202" target="_blank" rel="nofollow">Park Melvin A.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Rom?o Wanderson&option=202" target="_blank" rel="nofollow">Rom?o Wanderson;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Jaffé Rudolf&option=202" target="_blank" rel="nofollow">Jaffé Rudolf;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Fernandez‐Lima Francisco&option=202" target="_blank" rel="nofollow">Fernandez‐Lima Francisco;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Petroleomic and Forensic Chemistry Laboratory Department of ChemistryFederal University of Espírito Santo29075‐910 Vitória ES Brazil;</p> <p>Department of Chemistry and BiochemistryFlorida International UniversityMiami FL 33199 USA;</p> <p>Department of Chemistry and BiochemistryFlorida International UniversityMiami FL 33199 USA;</p> <p>Department of Chemistry and BiochemistryFlorida International UniversityMiami FL 33199 USA;</p> <p>Department of Chemistry and BiochemistryFlorida International UniversityMiami FL 33199 USA;</p> <p>Bruker Daltonics Inc.Billerica MA 01821 USA;</p> <p>Bruker Daltonics Inc.Billerica MA 01821 USA;</p> <p>Petroleomic and Forensic Chemistry Laboratory Department of ChemistryFederal University of Espírito Santo29075‐910 Vitória ES Brazil;</p> <p>Department of Chemistry and BiochemistryFlorida International UniversityMiami FL 33199 USA;</p> <p>Department of Chemistry and BiochemistryFlorida International UniversityMiami FL 33199 USA;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1187.html" title="分析化学">分析化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> </p> </li> <li> <span class="lefttit">入库时间</span> <span>2022-08-20 04:59:31</span> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704024020545.html">Coupling trapped ion mobility spectrometry 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R. </a> <span>1992</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：通过离子 - 分子反应动力学探测捕获的离子能量：傅里叶变换离子回旋共振质谱。</span> </p> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/academic-journal-cn_chinese-journal-family-planning_thesis/0201212618840.html">基质辅助激光解析/电离飞行时间质谱法和表面等离子谐振法在HPV分型检测中的应用比较</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=万敏&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 万敏</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=赵金银&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,赵金银</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=曲守方&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,曲守方</a> <span> <a href="/journal-cn-5578/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 中国计划生育学杂志 </a> </span> <span> . 2014</span><span>,第003期</span> </span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/academic-journal-cn_journal-chinese-mass-spectrometry-society_thesis/0201280103991.html">漂移时间离子淌度-四极杆-飞行时间串联质谱法分析寡糖同分异构体</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=吴启迪&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 吴启迪</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=谢成益&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,谢成益</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=俞建成&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,俞建成</a> <span> <a href="/journal-cn-8285/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 质谱学报 </a> </span> <span> . 2020</span><span>,第004期</span> </span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/academic-journal-cn_journal-anhui-agricultural-sciences_thesis/020121679672.html">微波消解-电感耦合等离子体直角加速飞行时间质谱法测定17种进出口卷烟中的10种金属元素</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=何杰&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 何杰</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=旦有明&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,旦有明</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=易建华&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,易建华</a> <span> <a href="/journal-cn-7281/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 安徽农业科学 </a> </span> <span> . 2013</span><span>,第013期</span> </span> </div> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/academic-journal-cn_rock-mineral-analysis_thesis/0201216545914.html">微波消解-直角加速飞行时间电感耦合等离子体质谱法测定烟叶中砷铅镉汞</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=何杰&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 何杰</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=曾千春&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,曾千春</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=旦有明&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,旦有明</a> <span> <a href="/journal-cn-7819/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 岩矿测试 </a> </span> <span> . 2012</span><span>,第003期</span> </span> </div> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-journal-cn_metallurgical-analysis_thesis/0201220557913.html">飞行时间-电感耦合等离子体质谱法测定钢、镍基合金及锆锡合金中痕量元素</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=GUSTAVSSON Ingemar&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 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mass spectrometry</a> <b>[P]</b> . <span> 外国专利：  US9129784B2 </span> <span> . 2015-09-08</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：傅立叶变换离子回旋共振质谱仪和富集离子的方法 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130419368166.html">FOURIER TRANSFORM ION CYCLOTRON RESONANCE MASS SPECTROMETER AND METHOD FOR CONCENTRATING IONS FOR FOURIER TRANSFORM ION CYCLOTRON RESONANCE MASS SPECTROMETRY</a> <b>[P]</b> . <span> 外国专利：  KR101239747B1 </span> <span> . 2013-03-06</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：傅立叶变换离子回旋共振质谱仪和富勒森变换离子回旋共振质谱仪中离子的浓缩方法 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130420822884.html">FOURIER TRANSFORM ION CYCLOTRON RESONANCE MASS SPECTROMETER AND METHOD FOR CONCENTRATING IONS FOR FOURIER TRANSFORM ION CYCLOTRON RESONANCE MASS SPECTROMETRY</a> <b>[P]</b> . <span> 外国专利：  US2013228681A1 </span> <span> . 2013-09-05</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：傅立叶变换离子回旋共振质谱仪和富勒森变换离子回旋共振质谱仪中离子的浓缩方法 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704024020545','4',7,2,1,'',this,24)" class="delivery" prompt="010401" title="通过人工服务将文献原文发送至邮箱" >获取原文</div> <div class="journalsub-pop-up" 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