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首页> 外文期刊>Angewandte Chemie >Separation of Xe from Kr with Record Selectivity and Productivity in Anion‐Pillared Ultramicroporous Materials by Inverse Size‐Sieving
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Separation of Xe from Kr with Record Selectivity and Productivity in Anion‐Pillared Ultramicroporous Materials by Inverse Size‐Sieving

机译：通过逆尺寸筛分将XE从KR与KR的选择性和生产率分离，通过逆尺寸筛分

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Abstract > The separation of xenon/krypton (Xe/Kr) mixture is of great importance to industry, but the available porous materials allow the adsorption of both, Xe and Kr only with limited selectivity. Herein we report an anion‐pillared ultramicroporous material NbOFFIVE‐2‐Cu‐i (ZU‐62) with finely tuned pore aperture size and structure flexibility, which for the first time enables an inverse size‐sieving effect in separation along with record Xe/Kr selectivity and ultrahigh Xe capacity. Evidenced by single‐crystal X‐ray diffraction, the rotation of anions and pyridine rings upon contact of larger‐size Xe atoms adapts cavities to the shape/size of Xe and allows strong host‐Xe interaction, while the smaller‐size Kr is excluded. Breakthrough experiments confirmed that ZU‐62 has a real practical potential for producing high‐purity Kr and Xe from air‐separation byproducts, showing record Kr productivity (206?mL?g ?1 ) and Xe productivity (42?mL?g ?1 , in desorption) as well as good recyclability. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 氙/氪（XE / KR）混合物的分离对工业具有重要意义，但可用的多孔材料仅允许吸附，XE和KR仅具有有限的选择性。在此，我们报告了一种阴离子柱柱柱的超微孔材料NBOFFIVE-2-CU-I（ZU-62），具有精细调谐的孔隙孔径和结构柔性，这是第一时间使得能够与记录XE的分离时的逆尺寸筛分效应。 KR选择性和超高XE容量。通过单晶X射线衍射证明，阴离子和吡啶环的旋转在较大尺寸的XE原子接触时适应腔的形状/尺寸并允许强大的主XE相互作用，而较小尺寸的KR被排除在外。突破性实验证实，Zu-62具有从空气分离副产物中生产高纯度Kr和XE的实际实际潜力，显示记录KR生产率（206？ml？g ？1 </ sup> ）和xe生产力（42？ml？g ？1 </ sup> 在解吸中以及良好的再循环性。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-19011/'>《Angewandte Chemie》</a> <b style="margin: 0 2px;">|</b><span>2020年第9期</span><b style="margin: 0 2px;">|</b><span>共6页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wang Qingju&option=202" target="_blank" rel="nofollow">Wang Qingju;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ke Tian&option=202" target="_blank" rel="nofollow">Ke Tian;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yang Lifeng&option=202" target="_blank" rel="nofollow">Yang Lifeng;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhang Zhaoqiang&option=202" target="_blank" rel="nofollow">Zhang Zhaoqiang;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Cui Xili&option=202" target="_blank" rel="nofollow">Cui Xili;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Bao Zongbi&option=202" target="_blank" rel="nofollow">Bao Zongbi;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ren Qilong&option=202" target="_blank" rel="nofollow">Ren Qilong;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yang Qiwei&option=202" target="_blank" rel="nofollow">Yang Qiwei;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Xing Huabin&option=202" target="_blank" rel="nofollow">Xing Huabin;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Key Laboratory of Biomass Chemical Engineering of ministry of EducationZhejiang UniversityHangzhou 310027 China;</p> <p>Key Laboratory of Biomass Chemical Engineering of ministry of EducationZhejiang UniversityHangzhou 310027 China;</p> <p>Key Laboratory of Biomass Chemical Engineering of ministry of EducationZhejiang UniversityHangzhou 310027 China;</p> <p>Key Laboratory of Biomass Chemical Engineering of ministry of EducationZhejiang UniversityHangzhou 310027 China;</p> <p>Key Laboratory of Biomass Chemical Engineering of ministry of EducationZhejiang UniversityHangzhou 310027 China;</p> <p>Key Laboratory of Biomass Chemical Engineering of ministry of EducationZhejiang UniversityHangzhou 310027 China;</p> <p>Key Laboratory of Biomass Chemical Engineering of ministry of EducationZhejiang UniversityHangzhou 310027 China;</p> <p>Key Laboratory of Biomass Chemical Engineering of ministry of EducationZhejiang UniversityHangzhou 310027 China;</p> <p>Key Laboratory of Biomass Chemical Engineering of ministry of EducationZhejiang UniversityHangzhou 310027 China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1188.html" title="应用化学">应用化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=adsorption&option=203" rel="nofollow">adsorption;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=anion-pillared materials&option=203" rel="nofollow">anion-pillared materials;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=gate-opening&option=203" rel="nofollow">gate-opening;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=xenon krypton separation&option=203" rel="nofollow">xenon krypton separation;</a> </p> <div class="translation"> 机译：吸附;阴离子柱材料;闸门开口;氙氪分离; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704028162587.html">Cover Picture: Separation of Xe from Kr with Record Selectivity and Productivity in Anion‐Pillared Ultramicroporous Materials by Inverse Size‐Sieving (Angew. 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target="_blank" rel="nofollow" class="tuijian_authcolor"> . 中国稀土学报 </a> </span> <span> . 1993</span><span>,第4期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-17542_thesis/020221853120.html">Xe-Kr 激光感生碰撞电离系统的初态研究</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . </a> <span> <a href="/conference-cn-17542/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 五省一市光学学会联合年会暨十三省市光学学会联合年会 </a> <span> <span> . 2008</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020315057537.html">Kr/Xe--CS体系势能面和束缚态能级的理论研究</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=段瑞&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 段瑞</a> <span> . 2019</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/061203856709.html">复杂裂变产物中Kr和Xe的快速分离系统及方法</a> <b>[P]</b> . <span> 中国专利： CN109939538B </span> <span> . 2020.07.28</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120100734077.html">复杂裂变产物中Kr和Xe的快速分离系统及方法</a> <b>[P]</b> . <span> 中国专利： CN109939538A </span> <span> . 2019-06-28</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130418196127.html">Metal-Organic Frameworks for Xe/Kr Separation</a> <b>[P]</b> . <span> 外国专利： <!-- 美国专利： --> US2014013943A1 </span> <span> . 2014-01-16</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：Xe / Kr分离的金属有机框架 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130418021687.html">Metal-organic frameworks for Xe/Kr separation</a> <b>[P]</b> . <span> 外国专利： <!-- 美国专利： --> US8784536B2 </span> <span> . 2014-07-22</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：Xe / Kr分离的金属有机框架 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130420621130.html">Metal-organic frameworks for Xe/Kr separation</a> <b>[P]</b> . <span> 外国专利： <!-- 美国专利： --> US8518153B2 </span> <span> . 2013-08-27</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：Xe / Kr分离的金属有机框架 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img 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