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Development of a new magnetic aluminum matrix nanocomposite

机译:开发新的磁铝基质纳米复合材料

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This article presents the results of a comparative investigation on microstructure, mechanical properties and magnetic characteristics of aluminum matrix nanocomposites reinforced with nickel ferrite nanoparticles. Magnetic nickel ferrite (NiFe2O4) nanoparticles with average size of 35 nm were synthesized via citrate-nitrate route and were used as the reinforcement phase in commercially pure aluminum matrix. Aluminum matrix samples with 0, 1, 2.5, 5 and 10 wt% ceramic reinforcement were fabricated using the powder metallurgy process. The sintered samples were then extruded at 400 degrees C to improve the density and homogeneity of the composite. Optical microscopy, SEM, FESEM, densitometry, XRD, DSC and VSM analyses were all used to evaluate the microstructure, porosity distribution, density, existing phases, possible reactions between the matrix and the reinforcements and magnetic properties of the samples. The results showed that the relative density of the composites decreased as the reinforcement weight percent was increased. The samples yield stress and ultimate tensile strength increased by increasing the weight percent of the reinforcement up to 5 wt%, however, they dropped at 10 wt% reinforcement content. The compressive yield stress, magnetization and coercivity of the composites were all observed to increase as the reinforcement content increased. However, the elongation of composite samples decreased considerably as the reinforcement content increased.
机译:本文介绍了用镍铁氧体纳米粒子增强的铝基质纳米复合材料的微观结构,机械性能和磁特性的比较研究结果。通过柠檬酸盐 - 硝酸盐途径合成磁镍铁氧体(NiFe2O4)纳米颗粒,其平均尺寸为35nm,并用作商业纯铝基中的增强相。使用粉末冶金工艺制造具有0,1,2.5,5和10wt%陶瓷增强件的铝基矩阵样品。然后将烧结样品在400℃下挤出,以提高复合材料的密度和均匀性。光学显微镜,SEM,FESEM,密度测定法,XRD,DSC和VSM分析均用于评估微观结构,孔隙率分布,密度,现有阶段,基质与样品的增强和磁性之间的可能反应。结果表明,随着增强重量百分比增加,复合材料的相对密度降低。通过将增强的重量百分比增加至5wt%,样品屈服应力和最终拉伸强度增加,但它们在10wt%的增强含量下降。随着增强含量的增加,复合材料的压缩屈服应力,磁化和矫顽力都被观察到增加。然而,随着增强型含量的增加,复合样品的伸长显着降低。

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