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Microstructure evolution and high temperature corrosion behavior of FeCrBSi coatings prepared by laser cladding

机译:激光熔覆制备FECRBSI涂层的微观结构演化和高温腐蚀行为

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摘要

In this study, an FeCrBSi coating was deposited on a stainless steel substrate by laser cladding with a 6 kW CO2 laser to improve the hardness and corrosion resistance. The phase composition, microstructure evolution and chemical composition of the coating were investigated via X-ray diffraction (XRD), confocal scanning laser microscopy (CSLM), scanning electron microscopy (SEM) and energy dispersive X-ray spectrometer (EDX). Microhardness and high temperature corrosion tests in molten aluminum were also conducted for evaluating the properties of the coating. The XRD pattern suggested that the coating was particularly composed of martensite, (Fe, Cr)(7)C-3 and CrFeB hard phases. The microstructure results exhibited that equiaxed dendrites, dendrite networks, columnar dendrites, cellular and planar grains were distributed from the surface to the bottom of the coating. The hardness of the substrate increased from 217 H-0.2 to 762 HV0.2. Moreover, the laser cladding FeCrBSi coating exhibited good corrosion resistance in molten aluminum, thereby making it a promising candidate in the surface modification and protection of hot dip aluminum equipment.
机译:在本研究中,通过用6 kW的CO2激光激光包层沉积在不锈钢基板上的Fecrbsi涂层,以提高硬度和耐腐蚀性。通过X射线衍射(XRD),共聚焦扫描激光显微镜(CSLM),扫描电子显微镜(SEM)和能量分散X射线光谱仪(EDX)研究了涂层的相组合物,微观结构演化和化学成分。还进行了熔融铝中的微硬度和高温腐蚀试验,用于评估涂层的性质。 XRD模式表明涂层特别由马氏体组成,(Fe,Cr)(7)C-3和CrFEB硬相。显微结构结果表明,从涂层底部分布了等轴的树突,树突网络,柱状树突,细胞和平面晶粒。基材的硬度从217 H-0.2至762 HV0.2增加。此外,激光熔覆Fecrbsi涂层在熔融铝中表现出良好的耐腐蚀性,从而使其成为热浸铝设备的表面改性和保护中的有希望的候选者。

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