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Electrochemical synthesis of polyaniline nanowires on Pt interdigitated microelectrode for room temperature NH _3 gas sensor application

机译:铂指叉微电极在室温NH _3气体传感器上电化学合成聚苯胺纳米线。

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摘要

In this work, we have successfully developed a facile and effective electrochemical route for directly growing polyaniline (PANI) nanowires (NWs) on platinum interdigitated microelectrode. The as-prepared NWs were characterized by field-emission scanning electron microscopy, transmission electron microscopy and Fourier-transform infrared spectroscopy. They revealed that the PANI NWs were obtained with diameters ranging from 50 to 200 nm and length up to hundreds of micro meters, depending on growth time. The as-obtained PANI NWs on the electrode exhibited a porous nature and the conducting emeraldine type structure. The gas sensing properties of PNAI NWs were explored by monitoring NH _3 in synthetic air in the concentration range of 25-500 ppm at room temperature. The results obtained demonstrated that PANI NWs have good potential as novel room temperature sensors for practical applications.
机译:在这项工作中,我们成功地开发了一种简便有效的电化学途径,用于在铂指状微电极上直接生长聚苯胺(PANI)纳米线(NWs)。通过场发射扫描电子显微镜,透射电子显微镜和傅立叶变换红外光谱对所制备的NW进行表征。他们发现,根据生长时间的不同,获得的PANI NW的直径范围为50到200 nm,长度可达数百微米。电极上如此获得的PANI NW表现出多孔性质和导电的翡翠型结构。通过在室温下监测浓度范围为25-500 ppm的合成空气中的NH_3,探索了PNAI NW的气敏特性。获得的结果表明,PANI NW作为实用的新型室温传感器具有良好的潜力。

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