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Impact of delignification on mechanical, morphological, and thermal properties of wood sawdust reinforced unsaturated polyester composites

机译:脱野对木锯末增强不饱和聚酯复合材料的机械,形态和热性能的影响

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摘要

Mechanical, morphological, and thermal properties of the raw and delignified wood sawdust (DWS) reinforced unsaturated polyester (UP) composites were evaluated. Composites were prepared using Resin Transfer molding technique by changing filler loading (5, 10, 15, and 20 wt%) for both raw and DWS reinforced UP. Mechanical (tensile and flexural), Fourier transform infrared spectroscopy (FTIR), morphological (scanning electron microscopy [SEM]) and thermal (thermogravimetric analysis [TGA]) properties were successively characterized. FTIR confirmed the removal of lignin from wood sawdust during the delignification process. The tensile strength, Young's modulus, and flexural strength values increased only up to 15% filler loading then decreased with increasing the filler. DWS reinforced composites had better mechanical properties compared to raw composites. SEM micrographs reveal that DWS reinforced composites have good compatibility with UP resin. According to TGA results, DWS reinforced composites showed enhanced thermal stability at the final decomposition stage above 400 degrees C. J. VINYL ADDIT. TECHNOL., 24:185-191, 2018. (c) 2016 Society of Plastics Engineers
机译:评估了原料和亚陀螺的木锯末(DWS)增强的不饱和聚酯(上)复合材料的机械,形态和热性能。使用树脂转移模塑技术通过改变填料加载(5,10,15和20wt%)来制备复合材料,用于加强加固的原料和DWS。傅里叶变换红外光谱(FTIR),形态学(扫描电子显微镜[SEM])和热(热重分析[TGA])性能,表征机械(抗拉和弯曲)。 FTIR在卖卖过程中证实从木锯末中除去木质素。拉伸强度,杨氏模量和弯曲强度值仅增加了15%的填充剂,随后随着填料的增加而降低。与原料复合材料相比,DWS增强复合材料具有更好的机械性能。 SEM显微照片揭示DWS增强复合材料与上树脂具有良好的相容性。根据TGA结果,DWS增强复合材料在最终分解阶段显示出高于400摄氏度的最终分解阶段的热稳定性。 Technol。,24:185-191,2018。(c)2016年塑料工程师协会

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