Electrospun polyethylene terephthalate/graphene oxide nanofibrous membrane followed by HPLC for the separation and determination of tamoxifen in human blood plasma

Sereshti Hassan; Bakhtiari Sadjad; Najarzadekan Hamid; Samadi Soheila

摘要

Abstract >An electrospun polyethylene terephthalate/graphene oxide nanofibrous mat was fabricated and used as an effective and novel membrane for the solid‐phase extraction of tamoxifen in human blood plasma samples before detection by high‐performance liquid chromatography. The membrane was characterized by some identification techniques, such as FTIR spectroscopy, X‐ray diffraction, and scanning electron microscopy. The effective variables of the extraction procedure including desorption condition (type and volume of the eluent), adsorbent dose, pH of sample solution, salt concentration, and sample loading time were investigated and their optimum values were obtained using one factor at a time methodology. Under the optimized conditions, the results showed wide linear concentration range of 5–2000?ng/mL with a determination coefficient of 0.992. The limits of detection and limits of quantification were 1.3 and 5.0?ng/mL, respectively. The intra‐day and inter‐day precisions were 3.4 and 4.6%, respectively. The method was successfully applied to determination of tamoxifen in the blood plasma samples and satisfactory relative recoveries (92.6–98.3 %) were achieved. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“main”> <标题类型=“main”>抽象</标题> >制造Electurpum聚对苯二甲酸丁酯/石墨烯氧化物纳米纤维垫，用作固相提取的有效和新的膜通过高效液相色谱检测前人血浆样品中的Tamoxifen。膜的特征在于一些识别技术，例如FTIR光谱，X射线衍射和扫描电子显微镜。研究包括解吸条件（洗脱液的类型和体积），吸附剂剂量，样品溶液的pH值，盐浓度和样品加载时间的有效变量，并在时间方法中使用一个因素获得它们的最佳值。在优化的条件下，结果显示宽线性浓度范围为5-2000〜Ng / mL，测定系数为0.992。定量检测限和限制分别为1.3和5.0？ng / ml。日内和日内的水平分别为3.4和4.6％。该方法成功地应用于血浆样品中三种毒素的测定，达到令人满意的相对回收（92.6-98.3％）。</ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" > 著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35800/'>《Journal of separation science. 》</a> <b style="margin: 0 2px;">|</b><span>2017年第17期</span><b style="margin: 0 2px;">|</b> <span>共9页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Sereshti Hassan&option=202" target="_blank" rel="nofollow">Sereshti Hassan;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Bakhtiari Sadjad&option=202" target="_blank" rel="nofollow">Bakhtiari Sadjad;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Najarzadekan Hamid&option=202" target="_blank" rel="nofollow">Najarzadekan Hamid;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Samadi Soheila&option=202" target="_blank" rel="nofollow">Samadi Soheila;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of Chemistry Faculty of ScienceUniversity of TehranTehran Iran;</p> <p>Department of Chemistry Faculty of ScienceUniversity of TehranTehran Iran;</p> <p>Department of Chemistry Faculty of ScienceUniversity of TehranTehran Iran;</p> <p>Department of Chemistry Faculty of ScienceUniversity of TehranTehran Iran;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li> <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span> <a href="https://www.zhangqiaokeyan.com/clc/159.html" title="化学">化学 ;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=electrospun nanofibers&option=203" rel="nofollow">electrospun nanofibers;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=high‐performance liquid chromatography&option=203" rel="nofollow">high‐performance liquid chromatography;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=human blood plasma&option=203" rel="nofollow">human blood plasma;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=membrane solid‐phase extraction&option=203" rel="nofollow">membrane solid‐phase extraction;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=tamoxifen&option=203" rel="nofollow">tamoxifen;</a> </p> <div class="translation"> 机译：Electrom 00纳米纤维;高效液相色谱;人血浆;膜固相萃取;Tamoxifen; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704025846814.html">Electrospun polyethylene terephthalate/graphene oxide nanofibrous membrane followed by HPLC for the separation and determination of tamoxifen in human blood plasma</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Sereshti Hassan&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Sereshti Hassan,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Bakhtiari Sadjad&option=202" target="_blank" rel="nofollow" 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href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=汪召豪&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,汪召豪</a> <span> <a href="/journal-cn-7621/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 武汉工程大学学报 </a> </span> <span> . 2013</span><span> ,第008期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-35113_thesis/020221240744.html">用ＨＰＬＣ测定对苯二甲酸二辛酯的方法研究</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=李素真&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 李素真</a> <span> <a href="/conference-cn-35113/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 第十次全国色谱学术报告会 </a> <span> <span> . 1995</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020314957420.html">石墨烯/聚对苯二甲酸乙二醇酯树脂的合成及其性能研究</a> <b>[A] </b> <span> <a 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translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：用于气体分离的氧化石墨烯纳米复合膜，还原型氧化石墨烯纳米复合膜及其制造方法 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130410014494.html">GRAPHENE OXIDE NANOCOMPOSITE MEMBRANE FOR GAS SEPARATION, REDUCED GRAPHENE OXIDE NANOCOMPOSITE MEMBRANE, AND METHOD FOR MANUFACTURING THE SAME</a> <b>[P]</b> . <span> 外国专利：  US2017014778A1 </span> <span> . 2017-01-19</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：用于气体分离的氧化石墨烯纳米复合膜，还原的氧化石墨烯纳米复合膜及其制造方法 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130414479006.html">GRAPHENE OXIDE NANOCOMPOSITE MEMBRANE FOR GAS SEPARATION, REDUCED GRAPHENE OXIDE NANOCOMPOSITE MEMBRANE, AND METHOD FOR MANUFACTURING SAME</a> <b>[P]</b> . 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