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Thiol‐ene click derived structurally well‐defined per(3,5‐dimethyl)phenylcarbamoylated cationic cyclodextrin separation material for achiral and chiral chromatography

机译：硫醇-NE点击衍生的每（3,5-二甲基）苯基氨基甲酰酯的阳离子环糊精分离材料，用于成立和手性色谱法

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Abstract > In this work, a novel single sulfoether‐bridged cationic per(3,5‐dimethyl)phenylcarbamoylated‐β‐cyclodextrin separation material was prepared by thiol‐ene click chemistry and characterized by using FTIR spectroscopy, solid‐state 13 C NMR spectroscopy and elemental analysis, which confirmed the correct structure. The separation material exhibited a good achiral separation performance for benzene homologues and phenylamine analogs, especially o ‐xylene and m ‐xylene, and m ‐phenylenediamine and o ‐phenylenediamine can be discriminated by the (3,5‐dimethyl)phenylcarbamoyl cyclodextrins. The chiral resolving ability of the separation material was evaluated by discriminating various isoxazolines, flavonoids, and β‐blockers in reversed‐phase high‐performance liquid chromatography. For isoxazolines, the material showed the best chiral discrimination toward 3‐aryl‐5‐(2‐oxopyrrolidin‐1‐yl)‐isoxazolines, where the resolution for 3ClPh‐OPr??reached 6.03. For flavonoids, it exhibited more efficient separation to the ones with more hydrophobic substituents, with a resolution of 5.93 for 6‐hydroxyflavanone. β‐Blockers were also enantioseparated satisfactorily on the material. The as‐prepared separation material is a good member of the thiol‐ene click derived cyclodextrin stationary phase family. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><abstract type =“main”xml：lang =“en”> <title type =“main”>抽象</ title> >在这项工作中，一个新的单硫醚桥阳离子（3,5-二甲基）通过硫醇-NEE键入化学制备苯基氨基甲酰胺-β-环糊精分离材料，并使用FTIR光谱法，固态 13-sup> c NMR光谱和元素分析来表征，证实了正确的结构。分离材料表现出苯同源物和苯胺类似物的良好的成立分离性能，尤其是 o℃和 mμl-亚胺，以及 m℃ - 苯二胺和 O </ i> - 苯二胺可以由（3,5-二甲基）苯基氨基酰基环糊精辨别。通过在反相高效液相色谱中鉴别各种异恶唑啉，黄酮类化合物和β-嵌体来评价分离材料的手性分辨能力。对于异恶唑啉，该材料显示出朝向3-芳基-5-（2-氧吡咯烷-1-基）-Sisoxazolines的最佳手性鉴别，其中用于3Clph-OPR的分辨率达到6.03。对于黄酮类化合物，它表现出与具有更多疏水性取代基的物质的高效分离，其分辨率为5.93对于6-羟基氟吡华酮。 β-嵌体也令人满意地对材料进行令人令人满意的。制备的分离材料是硫醇-NE的良好成员点击衍生的环糊精固定相家族。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35800/'>《Journal of separation science.》</a> <b style="margin: 0 2px;">|</b><span>2018年第13期</span><b style="margin: 0 2px;">|</b><span>共9页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Tang Xiaoying&option=202" target="_blank" rel="nofollow">Tang Xiaoying;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Xiaoxuan&option=202" target="_blank" rel="nofollow">Li Xiaoxuan;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Sun Yuwei&option=202" target="_blank" rel="nofollow">Sun Yuwei;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Xiao Yin&option=202" target="_blank" rel="nofollow">Xiao Yin;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wang Yong&option=202" target="_blank" rel="nofollow">Wang Yong;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Tianjin Key Laboratory of Molecular Optoelectronic Science Department of Chemistry School of ScienceTianjin UniversityTianjin China;</p> <p>Tianjin Key Laboratory of Molecular Optoelectronic Science Department of Chemistry School of ScienceTianjin UniversityTianjin China;</p> <p>School of Chemical Engineering and TechnologyTianjin UniversityTianjin China;</p> <p>Tianjin Key Laboratory of Molecular Optoelectronic Science Department of Chemistry School of ScienceTianjin UniversityTianjin China;</p> <p>Tianjin Key Laboratory of Molecular Optoelectronic Science Department of Chemistry School of ScienceTianjin UniversityTianjin China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/159.html" title="化学">化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=chiral stationary phases&option=203" rel="nofollow">chiral stationary phases;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=cyclodextrin&option=203" rel="nofollow">cyclodextrin;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=liquid chromatography&option=203" rel="nofollow">liquid chromatography;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=thiol‐ene click chemistry&option=203" rel="nofollow">thiol‐ene click chemistry;</a> </p> <div class="translation"> 机译：手性固定阶段;环糊精;液相色谱;硫醇-NE点击化学; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704025846504.html">Thiol‐ene click derived structurally well‐defined per(3,5‐dimethyl)phenylcarbamoylated cationic cyclodextrin separation material for achiral and chiral chromatography</a> 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href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=唐守万&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,唐守万</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=潘富友&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,潘富友</a> <span> <a href="/journal-cn-10803/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 分析测试学报 </a> </span> <span> . 2014</span><span>,第001期</span> </span> </div> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-journal-cn_detail_thesis/0201296600560.html">芳香醇异构体在纤维素-三(3,5-二甲基苯基氨基甲酸酯)色谱柱上的手性分离(英文)</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=吴旭日&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 吴旭日</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=范宇&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,范宇</a> <a 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href="/conference-cn-6752/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 西北地区第七届色谱学术报告会暨甘肃省第十二届色谱年会 </a> <span> <span> . 2012</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020314316693.html">L-α-氨基酸衍生物的合成与生物活性测定：（Ⅰ）：N-（5-邻氯苯基-2-呋喃甲酰氨基硫羰基）-L-α-氨基酸乙酯的合成与生物活性测定;（Ⅱ）：N-（5-邻氯苯基-2-呋喃甲酰基）甘氨酰胺衍生物的合成与生物活性测定;（Ⅲ）：N-（5-邻氯苯基-2-呋喃甲酰基）甘氨酰肼衍生物的合成与生物活性测定</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王庆东&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 王庆东</a> <span> . 2007</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120107308465.html">键合3,5-二甲基苯氨基甲酰化β-环糊精手性固定相在手性分析和/或分离盐酸舍曲林中间体(±)-Tetralone的应用</a> <b>[P]</b> . <span> 中国专利： CN104826619A </span> <span> . 2015-08-12</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120107991599.html">对甲/氯苯异氰酸酯修饰的阳离子环糊精手性拆分材料的点击制备及应用</a> <b>[P]</b> . <span> 中国专利： CN105498735A </span> <span> . 2016-04-20</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130401664602.html">CHROMATOGRAPHY MEMBRANES FORMED BY THIOL-ENE OR THIOL-YNE CLICK POLYMERIZATION REACTIONS</a> <b>[P]</b> . <span> 外国专利：  US2020047175A1 </span> <span> . 2020-02-13</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：硫醇或硫醇单击聚合反应形成的色谱膜 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130404680615.html">Chromatography membranes formed by thiol-ene or thiol-yne click polymerization reactions</a> <b>[P]</b> . <span> 外国专利：  US10357766B2 </span> <span> . 2019-07-23</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：硫醇-烯或硫醇-炔单击聚合反应形成的色谱膜 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130405430323.html">CHROMATOGRAPHY MEMBRANES FORMED BY THIOL-ENE OR THIOL-YNE CLICK POLYMERIZATION REACTIONS</a> <b>[P]</b> . <span> 外国专利：  EP3259050A4 </span> <span> . 2018-12-12</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：硫醇或硫醇单击聚合反应形成的色谱膜 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 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