Automated solid‐phase extraction of phenolic acids using layered double hydroxide–alumina–polymer disks

Ghani Milad; Palomino Cabello Carlos; Saraji Mohammad; Manuel Estela Jose; Cerdà Víctor; Turnes Palomino Gemma; Maya Fernando

摘要

Abstract > The application of layered double hydroxide–Al <sub>2</sub> O <sub>3</sub> –polymer mixed‐matrix disks for solid‐phase extraction is reported for the first time. Al <sub>2</sub> O <sub>3</sub> is embedded in a polymer matrix followed by an in situ metal‐exchange process to obtain a layered double hydroxide–Al <sub>2</sub> O <sub>3</sub> –polymer mixed‐matrix disk with excellent flow‐through properties. The extraction performance of the prepared disks is evaluated as a proof of concept for the automated extraction using sequential injection analysis of organic acids ( p ‐hydroxybenzoic acid, 3,4‐dihydroxybenzoic acid, gallic acid) following an anion‐exchange mechanism. After the solid‐phase extraction, phenolic acids were quantified by reversed‐phase high‐performance liquid chromatography with diode‐array detection using a core–shell silica–C18 stationary phase and isocratic elution (acetonitrile/0.5% acetic acid in pure water, 5:95, v/v). High sensitivity and reproducibility were obtained with limits of detection in the range of 0.12–0.25?μg/L (sample volume, 4?mL), and relative standard deviations between 2.9 and 3.4% (10?μg/L, n? =?6). Enrichment factors of 34–39 were obtained. Layered double hydroxide–Al <sub>2</sub> O <sub>3</sub> –polymer mixed‐matrix disks had an average lifetime of 50 extractions. Analyte recoveries ranged from 93 to 96% for grape juice and nonalcoholic beer samples. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> >分层双氢氧化物-al <sub> 2 </ sub> O <sub的应用>第一次报告了用于固相提取的3 </ sub> -polymer混合基质磁盘。 Al <sub> 2 </ sub> O <sub> 3 </ sub>嵌入聚合物基质中，然后嵌入原位金属交换过程中，得到层状双氢氧化物-Al <sub> 2 </ sub> o <sub> 3 </ sub> -polymer混合矩阵盘，具有出色的流通性能。准备好的盘的提取性能被评估为使用有机酸的顺序注射分析（ p </ i> - 羟基苯甲酸，3,4-二羟基苯甲酸，无碱酸）的顺序注射分析来评价概念证据阴离子交换机制。通过使用核 - 壳二氧化硅-C18固定相和等离子洗脱（纯水中乙腈/ 0.5％乙酸的二极管阵列检测，通过反相高效液相色谱法通过反相高效液相色谱法定量酚酸，用二极管阵列检测量化二极管阵列检测：95，v / v）。获得高灵敏度和再现性，在0.12-0.25Ω·μg/ l（样品体积，4×ml）的范围内，相对标准偏差在2.9和3.4％之间（10≤μg/ L， n ？</ i> =？6）。获得了34-39的富集因子。层状双氢氧化物-Al <亚> 2 </ sub> O <sub> 3 </ sub> -polymer混合基质磁盘的平均寿命为50萃取。葡萄汁和非酒精啤酒样品的分析物回收率范围为93至96％。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35800/'>《Journal of separation science.》</a> <b style="margin: 0 2px;">|</b><span>2018年第9期</span><b style="margin: 0 2px;">|</b><span>共8页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ghani Milad&option=202" target="_blank" rel="nofollow">Ghani Milad;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Palomino Cabello Carlos&option=202" target="_blank" rel="nofollow">Palomino Cabello Carlos;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Saraji Mohammad&option=202" target="_blank" rel="nofollow">Saraji Mohammad;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Manuel Estela Jose&option=202" target="_blank" rel="nofollow">Manuel Estela Jose;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Cerdà Víctor&option=202" target="_blank" rel="nofollow">Cerdà Víctor;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Turnes Palomino Gemma&option=202" target="_blank" rel="nofollow">Turnes Palomino Gemma;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Maya Fernando&option=202" target="_blank" rel="nofollow">Maya Fernando;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of ChemistryUniversity of the Balearic IslandsPalma de Mallorca Spain;</p> <p>Department of ChemistryUniversity of the Balearic IslandsPalma de Mallorca Spain;</p> <p>Department of ChemistryIsfahan University of TechnologyIsfahan Iran;</p> <p>Department of ChemistryUniversity of the Balearic IslandsPalma de Mallorca Spain;</p> <p>Department of ChemistryUniversity of the Balearic IslandsPalma de Mallorca Spain;</p> <p>Department of ChemistryUniversity of the Balearic IslandsPalma de Mallorca Spain;</p> <p>Department of ChemistryUniversity of the Balearic IslandsPalma de Mallorca Spain;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/159.html" title="化学">化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=automated sample treatment&option=203" rel="nofollow">automated sample treatment;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=high‐performance liquid chromatography&option=203" rel="nofollow">high‐performance liquid chromatography;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=layered double hydroxides&option=203" rel="nofollow">layered double hydroxides;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=phenolic acids&option=203" rel="nofollow">phenolic acids;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=solid‐phase extraction&option=203" rel="nofollow">solid‐phase extraction;</a> </p> <div class="translation"> 机译：自动样品处理;高效液相色谱;层状双氢氧化物;酚酸;固相提取; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704025846042.html">Automated solid‐phase extraction of phenolic acids using layered double hydroxide–alumina–polymer disks</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ghani Milad&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Ghani Milad,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Palomino Cabello Carlos&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Palomino Cabello Carlos,</a> <a 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L. </a> <span>2006</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：氢键酸性聚碳硅烷聚合物和固相微萃取在神经毒剂模拟物采集中的应用</span> </p> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/academic-journal-cn_materials-reports_thesis/0201275517141.html">阻燃聚合物/层状双氢氧化物复合材料的研究进展</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=丁鹏&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 丁鹏</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=唐圣福&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,唐圣福</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=汪庆&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,汪庆</a> <span> <a href="/journal-cn-7645/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 材料导报 </a> </span> <span> . 2012</span><span>,第005期</span> </span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/academic-journal-cn_materials-reports_thesis/0201211525330.html">阻燃聚合物/层状双氢氧化物复合材料的研究进展</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=丁鹏&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 丁鹏</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=唐圣福&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,唐圣福</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=汪庆&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,汪庆</a> <span> <a href="/journal-cn-7645/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 材料导报 </a> </span> <span> . 2011</span><span>,第005期</span> </span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/academic-journal-cn_materials-reports_thesis/0201275517074.html">阻燃聚合物/层状双氢氧化物复合材料的研究进展</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=丁鹏&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 丁鹏</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=唐圣福&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,唐圣福</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=汪庆&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,汪庆</a> <span> <a href="/journal-cn-7645/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 材料导报 </a> </span> <span> . 2011</span><span>,第003期</span> </span> </div> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/academic-journal-cn_detail_thesis/0201295552566.html">聚合物／层状双氢氧化物插层纳米复合材料及其制备方法</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . </a> <span> <a href="/journal-cn-56862/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 高分子材料科学与工程 </a> </span> <span> . 2006</span><span>,第6期</span> </span> </div> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-journal-cn_natural-science-progress_thesis/020125041240.html">聚合物/层状双氢氧化物纳米复合材料的研究与展望</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=瞿保钧&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 瞿保钧</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=陈伟&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,陈伟</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=邱龙臻&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,邱龙臻</a> <span> <a href="/journal-cn-5316/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 自然科学进展 </a> </span> <span> . 2005</span><span>,第003期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-3712_thesis/02022860450.html">聚合物/层状双氢氧化物纳米复合材料</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=CHEN Guangming&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . CHEN Guangming</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=陈光明&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,陈光明</a> <span> <a href="/conference-cn-3712/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 2014年全国高分子材料科学与工程研讨会 </a> <span> <span> . 2014</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020316339533.html">镁铝、锌铝层状双氢氧化物的改性及其在聚合物中的应用</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王少卿&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 王少卿</a> <span> . 2016</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120107715050.html">选择性地吸附不饱和脂肪酸的层状双氢氧化物及使用了该层状双氢氧化物的化妆品</a> <b>[P]</b> . <span> 中国专利： CN105209389A </span> <span> . 2015-12-30</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120103410394.html">磁性层状双氢氧化物的制备方法、磁性层状双氢氧化物及其应用</a> <b>[P]</b> . <span> 中国专利： CN110898796A </span> <span> . 2020-03-24</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130413179802.html">Cesium-containing layered double hydroxide complex, waste solidified body, the processing method of the cesium-containing wastewater, layered double hydroxide complex, and method of manufacturing a layered double hydroxide complex</a> <b>[P]</b> . <span> 外国专利：  JP5936196B2 </span> <span> . 2016-06-22</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：含铯的层状双氢氧化物络合物，废固化物，含铯废水的处理方法，层状双氢氧化物络合物和层状双氢氧化物络合物的制造方法 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130425483530.html">process for recovering aluminum hydroxide crystals from a turgid bayer process liquor by adding a crystallization modifier to the liquor, an improved process for the production of aluminum hydroxide from a bayer process liquor containing an aqueous phase of sodium aluminate and the liquor is produced by the separation of suspended solids insoluble in caustics, improved crystallization modifier composition for the production of aluminum hydroxide by the bayer process, bayer process to produce aluminum hydroxide crystals which have a reduced formation of fines of the simultaneous product with an upward shift in the aluminum hydroxide particle size distribution without a substantial reduction in the total yield of the aluminum hydroxide product and aluminum hydroxide crystals "</a> <b>[P]</b> . <span> 外国专利：  BRPI0613815A2 </span> <span> . 2011-02-15</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：通过在液体中加入结晶改性剂从节水拜耳法液体中回收氢氧化铝晶体的方法，一种改进的从包含铝酸钠水相的拜耳法液体中生产氢氧化铝的方法，该液体通过分离得到不溶于苛性碱的悬浮固体，通过拜耳法生产氢氧化铝的改进的结晶改性剂组合物，拜耳法生产氢氧化铝晶体的方法，减少了同时产物的细粉形成，氢氧化铝颗粒尺寸向上移动氢氧化铝产物和氢氧化铝晶体的总收率没有明显降低的分布” </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130410952510.html">LAYERED DOUBLE HYDROXIDE CAPABLE OF ADSORBING UNSATURATED FATTY ACIDS SELECTIVELY, AND COSMETIC PRODUCED USING SAID LAYERED DOUBLE HYDROXIDE</a> <b>[P]</b> . <span> 外国专利：  EP2998274A4 </span> <span> . 2017-03-15</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：能够选择性吸附不饱和脂肪酸的层状双氢氧化物，以及使用所述层状双氢氧化物生产的化妆品 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img 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