Experimental study on spontaneous imbibition of recycled fracturing flow-back fluid to enhance oil recovery in low permeability sandstone reservoirs

摘要

In light of the high treatment costs for massive amounts of fracturing flow-back fluid and its harmfulness to the environment, a novel method of recycled fracturing flow-back fluid (RFFF) to enhance oil recovery by spontaneous imbibition is proposed in this study; this method does not allow the flow-back fluid back to the ground, thereby preventing negative impacts. The wettability alteration and interfacial tension (IFT) can effectively strengthen the spontaneous imbibition to enhance oil recovery in low-permeability sandstone reservoirs. This study combines the effects of wettability alteration and IFT with the use of the RFFF, which is composed of viscoelastic surfactants, on the spontaneous imbibition in low-permeability outcrop cores. Contact angle (CA) experiments, IFT experiments, and spontaneous imbibition experiments are conducted. The CA and IFT experimental results showed that the RFFF solutions changed the wettability of the core surface from oil-wet to waterwet and easily reduced the IFT between the crude oil and the RFFF solution to 10(-3)-10(-2) mN/m, which improved the oil recovery by changing the capillary forces. The spontaneous imbibition results showed that the RFFF solutions at concentrations of 0.03 - 0.10 wt% resulted in a higher imbibition recovery due to the synergistic effect of the wettability alteration and the IFT, which was attributed to the wedge film structure and the spreading force. It can be concluded that the use of the RFFF has the potential to further enhance oil recovery after fracturing the formation in low-permeability reservoirs without letting the fluid flow back to the ground. The proposed method is multi-functional and does not only improve the oil recovery by integrating fracturing and displacement methods but also reduces the costs of reservoir development and protects the environment.