Electrical and melt rheological characterization of PC and co‐continuous PC/SAN blends filled with CNTs: Relationship between melt‐mixing parameters, filler dispersion, and filler aspect ratio

Liebscher Marco; Domurath Jan; Krause Beate; Saphiannikova Marina; Heinrich Gert; P?tschke Petra

摘要

ABSTRACT > Electrical and melt rheological properties of melt‐mixed polycarbonate (PC) and co‐continuous PC/poly(styrene–acrylonitrile) (SAN) blends with carbon nanotubes (CNTs) are investigated. Using two sets of mixing parameters, different states of filler dispersion are obtained. With increasing CNT dispersion, an increase in electrical resistivity near the percolation threshold of PC–CNT composites and (PC?+?CNT)/SAN blends is observed. This suggests that the higher mixing energies required for better dispersion also result in a more severe reduction of the CNT aspect ratio; this effect was proven by CNT length measurements. Melt rheological studies show higher reinforcing effects for composites with worse dispersion. The Eilers equation, describing the melt viscosity as function of filler content, was used to fit the data and to obtain information about an apparent aspect ratio change, which was in accordance with measured CNT length reduction. Such fitting could be also transferred to the blends and serves for a qualitatively based discussion. ? 2017 Wiley Periodicals, Inc. J. Polym. Sci., Part B: Polym. Phys. 2018 , 56 , 79–88 </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract XMLNS =“http://www.wiley.com/namespaces/wiley”type =“main”> <title type =“main”>摘录</ title> >熔融混合的电气和熔体流变性质研究了聚碳酸酯（PC）和共连续的PC / Poly（苯乙烯 - 丙烯腈）（SAN）与碳纳米管（CNT）共混物。使用两组混合参数，获得不同的填充分散状态。随着CNT分散的增加，观察到PC-CNT复合材料的渗透阈值附近的电阻率和（PC？+β+ CNT）/ SAN混合物的增加。这表明更好的分散性所需的更高的混合能量也导致CNT纵横比的更严重降低;通过CNT长度测量证明了这种效果。熔体流变学研究表明复合材料具有更差的分散体的增强效果。描述了作为填料含量的函数的熔体粘度的EiLer方程用于拟合数据并获得关于表观纵横比变化的信息，这是根据测量的CNT长度减少的变化。这种配件也可以转移到混合中并用于基于定性的讨论。还2017年Wiley期刊，Inc.J.Minon。 SCI。，B部分：聚合物。物理。 2018 </ b>， 56 </ i>，79-88 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35627/'>《Journal of Polymer Science, Part B. Polymer Physics》</a> <b style="margin: 0 2px;">|</b><span>2018年第1期</span><b style="margin: 0 2px;">|</b><span>共10页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liebscher Marco&option=202" target="_blank" rel="nofollow">Liebscher Marco;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Domurath Jan&option=202" target="_blank" rel="nofollow">Domurath Jan;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Krause Beate&option=202" target="_blank" rel="nofollow">Krause Beate;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Saphiannikova Marina&option=202" target="_blank" rel="nofollow">Saphiannikova Marina;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Heinrich Gert&option=202" target="_blank" rel="nofollow">Heinrich Gert;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=P?tschke Petra&option=202" target="_blank" rel="nofollow">P?tschke Petra;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Leibniz‐Institut für Polymerforschung Dresden e.V. (Leibniz Institute of Polymer Research Dresden IPF) Hohe Str. 6Dresden D‐01069 Germany;</p> <p>Leibniz‐Institut für Polymerforschung Dresden e.V. (Leibniz Institute of Polymer Research Dresden IPF) Hohe Str. 6Dresden D‐01069 Germany;</p> <p>Leibniz‐Institut für Polymerforschung Dresden e.V. (Leibniz Institute of Polymer Research Dresden IPF) Hohe Str. 6Dresden D‐01069 Germany;</p> <p>Leibniz‐Institut für Polymerforschung Dresden e.V. (Leibniz Institute of Polymer Research Dresden IPF) Hohe Str. 6Dresden D‐01069 Germany;</p> <p>Leibniz‐Institut für Polymerforschung Dresden e.V. (Leibniz Institute of Polymer Research Dresden IPF) Hohe Str. 6Dresden D‐01069 Germany;</p> <p>Leibniz‐Institut für Polymerforschung Dresden e.V. (Leibniz Institute of Polymer Research Dresden IPF) Hohe Str. 6Dresden D‐01069 Germany;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1185.html" title="高分子化学（高聚物）">高分子化学（高聚物）;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=carbon nanotubes&option=203" rel="nofollow">carbon nanotubes;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=electrical properties&option=203" rel="nofollow">electrical properties;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=morphology&option=203" rel="nofollow">morphology;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=nanocomposites&option=203" rel="nofollow">nanocomposites;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=rheology&option=203" rel="nofollow">rheology;</a> </p> <div class="translation"> 机译：碳纳米管;电学性质;形态;纳米复合材料;流变学; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704025811030.html">Electrical and melt rheological characterization of PC and co‐continuous PC/SAN blends filled with CNTs: Relationship between melt‐mixing parameters, filler dispersion, and filler aspect ratio</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liebscher Marco&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Liebscher Marco,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Domurath Jan&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Domurath Jan,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Krause Beate&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Krause Beate,</a> <a href="/journal-foreign-35627/" target="_blank" rel="nofollow" class="tuijian_authcolor">Journal of Polymer Science, Part B. 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href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=吴书航&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 吴书航</a> <span> . 2020</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06130459874775.html">Polyarylene sulphide blend with spherical filler and opt. di:sulphide - used as thermoplastic encapsulating compsn., esp. for electronic device, with lower melt viscosity than blend filled with aspherical filler</a> <b>[P]</b> . <span> 外国专利：  DE4228133A1 </span> <span> . 1994-03-03</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：聚芳硫醚与球形填料的共混物。 di：硫化物-用作热塑性封装材料，特别是用于电子设备，其熔融粘度比填充非球面填料的共混料低 </span> </p> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06130464827151.html">PREPARATION OF CONTROLLED ATMOSPHERE PACKAGING FILMS BY MELT BLENDING POLYMER/FILLER MIXTURE HAVING PREDETERMINED MOISTURE CONTENT AND STRETCHING THE RESULTANT CAST FILM IN ONE DIMENSION BY A FACTOR OF AT LEAST TWO</a> <b>[P]</b> . <span> 外国专利：  NZ226480A </span> <span> . 1990-12-21</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：通过具有预定水分含量的熔融共混聚合物/填充剂混合物并通过至少两个因素拉伸一维结果成膜薄膜来制备可控气氛包装薄膜 </span> </p> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130462841555.html">Continuous prodn. of powder paints - by mixing binder and hardener, feeding into extruder, adding premixed fillers, pigments etc. to the melt, extruding, cooling and crushing</a> <b>[P]</b> . <span> 外国专利：  DE4101048A1 </span> <span> . 1992-07-23</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：连续产品粉末涂料的生产-通过混合粘合剂和硬化剂，加入到挤出机中，将预混合的填料，颜料等添加到熔体中，挤出，冷却和粉碎 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704025811030','4',7,2,1,'',this,24)" class="delivery" prompt="010401" title="通过人工服务将文献原文发送至邮箱" >获取原文</div> <div class="journalsub-pop-up" style="display: none"> <div class="journal-sub"> <h2>期刊订阅</h2> <img src="https://cdn.zhangqiaokeyan.com/img/loginclose.png" alt="关闭" onclick="$('.journalsub-pop-up').hide()"> <p class="pardon">抱歉，该期刊暂不可订阅，敬请期待！</p> <p class="current">目前支持订阅全部北京大学中文核心（2020）期刊目录。</p> <div style="display: flex;margin-top: 69px;justify-content: 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