Microwave-enhanced, solvent-free synthesis of singly and doubly C-labelled trans-cinnamic acid at the alpha- and beta-carbon positions

Guibin Ma; Sophia E. Hayes

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Microwave-enhanced, solvent-free synthesis of singly and doubly C-labelled trans-cinnamic acid at the alpha- and beta-carbon positions

机译：微波增强，无溶剂的合成在α-和β-碳位置的单独和双C标记的反肉桂酸的单独和双C-标记的反肉桂酸

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摘要

~(13)C-labelled trans-cinnamic acid (3-phenyl-2-propenoic acid) has been synthesized in one step using benzaldehyde-carbonyl-~(13)C and malonic acid-2-~(13)C in the presence of ammonium acetate under microwave irradiation and solvent-free conditions.

机译：〜（13）C-标记的反式肉桂酸（3-苯基-2-丙酸）在一步中使用苯甲醛 - 羰基 - 〜（13）C和丙酸-2-〜（13）C合成在微波辐射和无溶剂条件下存在乙酸铵。

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来源
《Journal of Labelled Compounds and Radiopharmaceuticals》 |2004年第12期|共7页
作者
Guibin Ma; Sophia E. Hayes;
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作者单位

Department of Chemistry Washington University in St. Louis St. Louis MO 63130-4899 USA;

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原文格式 PDF
正文语种 eng
中图分类药学;
关键词
trans-cmnamic acid; 3-phenyl-2-propenoic acid; ~(13)C label; solid-phase reaction; microwave synthesis;

机译：反式cmnamic酸;3-苯基-2-丙酸;〜（13）C标签;固相反应;微波合成;
入库时间 2022-08-20 09:30:09

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1. Microwave-enhanced, solvent-free synthesis of singly and doubly C-labelled trans-cinnamic acid at the alpha- and beta-carbon positions [J] . Guibin Ma, Sophia E. Hayes Journal of Labelled Compounds and Radiopharmaceuticals . 2004,第12期

机译：微波增强，无溶剂的合成在α-和β-碳位置的单独和双C标记的反肉桂酸的单独和双C-标记的反肉桂酸
2. Singly, Doubly, and Triply Linked Corrole Oligomers: Synthesis, Structures, and Linking Position Dependent Properties [J] . Ooi Shota, Ueta Kento, Tanaka Takayuki, ChemPlusChem . 2019,第6期

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3. The photodimerisation of the alpha- and beta-forms of trans-cinnamic acid: a study of single crystals by vibrational microspectroscopy [J] . Atkinson SDM., Almond MJ., Hollins P., Spectrochimica acta, Part A. Molecular and biomolecular spectroscopy . 2003,第3期

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Microwave-enhanced, solvent-free synthesis of singly and doubly C-labelled trans-cinnamic acid at the alpha- and beta-carbon positions

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