Salting‐out extraction of sinomenine from <fi xmlns='http://www.wiley.com/namespaces/wiley'>Sinomenium acutum</fi>Sinomenium acutum by an alcohol/salt aqueous two‐phase system using ionic liquids as additives

Li Fenfang; Li Qiao; Wu Shuanggen; Sun Danyu; Tan Zhijian

摘要

Abstract <section xml:id="jctb5318-sec-0001" numbered="no"> <title type="main">BACKGROUND xml:id="jctb5318-para-0001"> The aqueous two‐phase extraction ( <fc>ATPE</fc> ) based on organic solvent and inorganic salt was considered a promising method in the extraction, enrichment, and purification field. Ionic liquids ( <fc>ILs</fc> ) used as additives to the aqueous two‐phase system ( <fc>ATPS</fc> ) can improve the extraction yield. </section> <section xml:id="jctb5318-sec-0002" numbered="no"> <title type="main">RESULTS xml:id="jctb5318-para-0002"> In this study, seven <fc>ILs</fc> were added to the ethanol/ammonium sulfate <fc>ATPS</fc> and used for the salting‐out extraction ( <fc>SOE</fc> ) of sinomenine from <fi>Sinomenium acutum</fi> . The <fc>IL</fc> [ <fc> C <sub>2</sub> OHmim </fc> ] <fc> FeCl <sub>4</sub> </fc> was screened as the optimal additive, then the influencing factors <fc>IL</fc> amount, ethanol concentration, salt concentration, and temperature were investigated. The maximum extraction efficiency of 96.4% was obtained under the following conditions: 23.06?wt% ethanol concentration, 27.28?wt% ( <fc> NH <sub>4</sub> </fc> ) <fc> <sub>2</sub> SO <sub>4</sub> </fc> concentration, 4.0?wt% [ <fc> C <sub>2</sub> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><abstract xmlns =“http://www.wiley.com/namespaces/wiley”type =“main”xml：id =“JCTB5318-ABS-0001”> <标题类型=“main”>抽象</ title> < XML部分：ID =“JCTB5318-SEC-0001”编号=“否”> <标题类型=“main”>背景</ title> XML：ID =“JCTB5318-PARA-0001”>水性两阶段基于有机溶剂和无机盐的萃取（<FC> ATPE </ FC>）被认为是提取，富集和纯化领域的有希望的方法。用作两相系统水溶液（<Fc> ATPS </ Fc>）的添加剂可以提高萃取产率的离子液体（<Fc> ILS </ Fc>）。 </ p> </ section> <section XML：ID =“JCTB5318-SEC-0002”编号=“否”> <标题类型=“main”>结果</ title> XML：ID =“JCTB5318-PARA在本研究中，将七个<Fc> ILS </ Fc>加入到乙醇/硫酸铵<Fc> ATPS </ Fc>中，并用于腌制萃取（<Fc> SOE </ Fc> ）来自<fi> simomenium acutum的sinomenine </ fi>。 <Fc> IL </ FC> [<FC> C <sub> 2 </ sub> OHMIM </ fc>] <FC> FECL <SUB> 4 </ sub> </ Fc>被筛选为最佳添加剂然后研究了影响因素<Fc> IL </ Fc>量，乙醇浓度，盐浓度和温度。在以下条件下获得96.4％的最大提取效率：23.06℃乙醇浓度，27.28〜wt％（<Fc> NH <sub> 4 </ sub> </ Fc>）<Fc> <sub> 2 </ sub> SO <sub> 4 </ sub> </ fc>浓度，4.0≤wt％[<fc> c <sub> 2 </ sub> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-33908/'>《Journal of Chemical Technology & Biotechnology》</a> <b style="margin: 0 2px;">|</b><span>2018年第7期</span><b style="margin: 0 2px;">|</b><span>共6页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Fenfang&option=202" target="_blank" rel="nofollow">Li Fenfang;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Qiao&option=202" target="_blank" rel="nofollow">Li Qiao;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wu Shuanggen&option=202" target="_blank" rel="nofollow">Wu Shuanggen;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Sun Danyu&option=202" target="_blank" rel="nofollow">Sun Danyu;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Tan Zhijian&option=202" target="_blank" rel="nofollow">Tan Zhijian;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>College of Chemistry and Chemical EngineeringCentral South UniversityChangsha China;</p> <p>College of Chemistry and Chemical EngineeringCentral South UniversityChangsha China;</p> <p>College of Chemistry and Chemical EngineeringCentral South UniversityChangsha China;</p> <p>College of Chemistry and Chemical EngineeringCentral South UniversityChangsha China;</p> <p>Institute of Bast Fiber Crops and Center of Southern Economic CropsChinese Academy of Agricultural SciencesChangsha China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/180.html" title="生物工程学（生物技术）">生物工程学（生物技术）;</a><a href="https://www.zhangqiaokeyan.com/clc/20827.html" title="生物化学过程">生物化学过程;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=aqueous two‐phase system&option=203" rel="nofollow">aqueous two‐phase system;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=salting‐out extraction&option=203" rel="nofollow">salting‐out extraction;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ionic liquids&option=203" rel="nofollow">ionic liquids;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=sinomenine&option=203" rel="nofollow">sinomenine;</a> </p> <div class="translation"> 机译：两相系统;腌制萃取;离子液体;SINOMENINE; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> 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Salting‐out extraction of sinomenine from Sinomenium acutumSinomenium acutum by an alcohol/salt aqueous two‐phase system using ionic liquids as additives

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