beta-SELECTIVE D-PSICOFURANOSYLATION OF PYRIMIDINE BASES AND THIOLS

Ueda Atsushi; Nishimura Yuri; Makura Yui; Tanaka Masakazu; Uenishi Junichi

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beta-SELECTIVE D-PSICOFURANOSYLATION OF PYRIMIDINE BASES AND THIOLS

机译：β-选择性D-吡啶基碱基和硫醇的psicofuranysylation

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N-Glycosidation of D-psicofuranosyl donor 1 with pyrimidine bases took place beta-selectively in a beta/alpha -ratio of 8:1 similar to 7:1. For S-glycosidation, 3,4-O-(3-pentylidene)-protected D-psicofuranosyl donor 15 was effective to increase beta-selectivity up to 7:1.

机译：用嘧啶碱基的D-哌啶呋喃糖基供体1的N-糖苷化在类似于7：1的β/α-RATIO中选择性地进行β-选择性地进行β-选择性。对于S-糖苷化，3,4-O-（3-四戊二烯） - 保护的D-雌脲呋喃糖基供体15可有效地将β选择性增加至7：1。

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《Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry 》 |2018年第2期| 共15页
作者
Ueda Atsushi; Nishimura Yuri; Makura Yui; Tanaka Masakazu; Uenishi Junichi;
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作者单位

Kyoto Pharmaceut Univ Yamashina Ku Kyoto 6078412 Japan;

Kyoto Pharmaceut Univ Yamashina Ku Kyoto 6078412 Japan;

Nagasaki Univ Grad Sch Biomed Sci 1-14 Bunkyo Machi Nagasaki 8528521 Japan;

Nagasaki Univ Grad Sch Biomed Sci 1-14 Bunkyo Machi Nagasaki 8528521 Japan;

Kyoto Pharmaceut Univ Yamashina Ku Kyoto 6078412 Japan;

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正文语种 eng
中图分类化学 ;
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1. 利用氯化胆碱基低共熔溶剂从氧化锌烟尘中选择性回收锌 [J] . 朱啸林, 徐存英, 唐杰, 中国有色金属学报：英文版 . 2019 ,第010期
2. 利用氯化胆碱基低共熔溶剂从氧化锌烟尘中选择性回收锌 [J] . 朱啸林, 徐存英, 唐杰, 中国有色金属学报（英文版） . 2019 ,第010期
3. beta-SELECTIVE D-PSICOFURANOSYLATION OF PYRIMIDINE BASES AND THIOLS [J] . Ueda Atsushi, Nishimura Yuri, Makura Yui, Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry . 2018 ,第2期

机译：β-选择性D-吡啶基碱基和硫醇的psicofuranysylation
4. Toward Perfect Regiocontrol for beta-Selective Cyclopolymerization Using a Ru-Based Olefin Metathesis Catalyst [J] . Jung Kijung, Kim Kunsoon, Sung Jong-Chan, Macromolecules . 2018 ,第12期

机译：使用Ru基烯烃复分解催化剂对β选择性环聚合的完美regiocontrol
5. Synthesis of new organochalcogen (Se or Te) based multifunctional pyrimidine derivatives: X-ray structure determination of 2,4-bis (arylchalcogenyl)pyrimidine and 2-chloro-4,6-bis(arylchalcogenyl) pyrimidine compounds [J] . Ekta Arora, K.K. Bhasin, S.K. Mehta, Polyhedron: The International Journal for Inorganic and Organometallic Chemistry . 2014 ,第Null期

机译：新的基于有机硫属元素（Se或Te）的多功能嘧啶衍生物的合成：2,4-双（芳基硫属酰基）嘧啶和2-氯-4,6-双（芳基硫属酰基）嘧啶化合物的X射线结构测定
6. Free Radical Reactions in the System Thiol/Pyrimidine [C] . A. Wojcik, S. Naumov, B. Marciniak, International Society for Free Radical Research . 2006

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7. Design and Synthesis of Pyrimidine Based Heterocycles as Potential Anti-cancer Agents with Combination Chemotherapeutic Potential or Targeted One Carbon Metabolism Inhibition and Anti-opportunistic Agents [D] . Doshi, Arpit. 2019

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8. Heterocyclization of polarized system: synthesis antioxidant and anti-inflammatory 4-(pyridin-3-yl)-6-(thiophen-2-yl) pyrimidine-2-thiol derivatives [O] . Wesam S. Shehab, Magda H. Abdellattif, Samar M. Mouneir 2018

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9. Copper mediated coupling of 2-(piperazine)-pyrimidine iodides with aryl thiols using Cu(I)thiophene-2-carboxylate [O] . Liza Shrestha, Hardik J. Patel, Yanlong Kang, 2017

机译：铜介导的2-（哌嗪） - 吡啶胺碘化物与芳基硫醇使用Cu（I）噻吩-2-羧酸酯

beta-SELECTIVE D-PSICOFURANOSYLATION OF PYRIMIDINE BASES AND THIOLS

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