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Synthesis and characterization of multi-wall carbon nanotubes/DLC incorporated composites as electrode materials for supercapacitor

机译:多壁碳纳米管/ DLC掺入复合材料的合成与表征作为超级电容器的电极材料

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摘要

In this work, MWCNTs were synthesized by ACVD technique on the Cu substrate surface coated by DLC film prepared by radio frequency (RF) plasma treatment at the power of 50, 100 and 150 W in order to find the optimum conditions for MWCNTs to be utilized as an electrode material of a supercapacitor. Field Emission Scanning Electron Microscopy (FE-SEM) was employed in the characterization of the obtained MWCNTs. It was found that the MWCNTs grown on DLC film prepared at the plasma power of 100 W gave the highest percentage of carbon yield (188%), whereas the results from the Electrochemical Impedance Spectrometry (EIS) study showed that when used as an electrode of a supercapacitor, the MWCNT grown on DLC film prepared at the plasma power of 150 W yielded the highest parasitic capacitance of 421 mu F/cm(2).
机译:在这项工作中,通过在50,100和150w的功率下通过射频(RF)等离子体处理的DLC膜涂覆的Cu衬底表面上的ACVD技术合成MWCNT,以便找到用于使用MWCNT的最佳条件 作为超级电容器的电极材料。 现场发射扫描电子显微镜(Fe-SEM)用于所获得的MWCNT的表征。 发现在100W的等离子体功率下制备的DLC膜上生长的MWCNT含量最高(188%),而电化学阻抗光谱(EIS)的结果表明,当用作电极时 超级电容器,在150W的等离子体功率下制备的DLC膜上生长的MWCNT产生了421μF/ cm(2)的最高寄生电容。

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